Acetic acid (S)-1-[2-((1S,6R)-2,2,6-trimethyl-cyclohexyl)-ethyl]-butyl ester

Base Information

Chemical Name:Acetic acid (S)-1-[2-((1S,6R)-2,2,6-trimethyl-cyclohexyl)-ethyl]-butyl ester
CAS No.:253454-26-1
Molecular Formula:C₁₇H₃₂O₂
Molecular Weight:268.44
Hs Code.:

Synonyms:Acetic acid (S)-1-[2-((1S,6R)-2,2,6-trimethyl-cyclohexyl)-ethyl]-butyl ester

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Chemical Property of Acetic acid (S)-1-[2-((1S,6R)-2,2,6-trimethyl-cyclohexyl)-ethyl]-butyl ester

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Technology Process of Acetic acid (S)-1-[2-((1S,6R)-2,2,6-trimethyl-cyclohexyl)-ethyl]-butyl ester

There total 12 articles about Acetic acid (S)-1-[2-((1S,6R)-2,2,6-trimethyl-cyclohexyl)-ethyl]-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65562-82-5
8,12-dimethyltrideca-5,7,11-trien-4-one

: 253454-26-1
Acetic acid (S)-1-[2-((1S,6R)-2,2,6-trimethyl-cyclohexyl)-ethyl]-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 68 percent / H₃PO₄ / 0.67 h / 20 °C

2: 93 percent / NaBH₄ / methanol / 0 °C

3: H₂ / Pd/C / acetic acid / 20 °C / 2280 Torr

4: pyridine / CH₂Cl₂

5: dimethylformamide / Heating

With pyridine; sodium tetrahydroborate; phosphoric acid; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; 1: Cyclization / 2: Hydrogenation / 3: Catalytic hydrogenation / 4: Tosylation / 5: Acetylation;
DOI:10.1002/(SICI)1522-2675(19991006)82:10<1762::AID-HLCA1762>3.0.CO;2-1

Reference yield:

: 70092-19-2
(+/-)-1-(2,6,6-trimethylcyclohex-2-enyl)hex-1-en-3-one

: 253454-26-1
Acetic acid (S)-1-[2-((1S,6R)-2,2,6-trimethyl-cyclohexyl)-ethyl]-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / NaBH₄ / methanol / 0 °C

2: H₂ / Pd/C / acetic acid / 20 °C / 2280 Torr

3: pyridine / CH₂Cl₂

4: dimethylformamide / Heating

With pyridine; sodium tetrahydroborate; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; 1: Hydrogenation / 2: Catalytic hydrogenation / 3: Tosylation / 4: Acetylation;
DOI:10.1002/(SICI)1522-2675(19991006)82:10<1762::AID-HLCA1762>3.0.CO;2-1

Reference yield:

: (1E)-1-(trans-2,2,6-Trimethylcyclohexyl)-1-hexen-3-on

: 253454-26-1
Acetic acid (S)-1-[2-((1S,6R)-2,2,6-trimethyl-cyclohexyl)-ethyl]-butyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 95 percent / NaBH₄ / methanol; CH₂Cl₂

2: 41 percent / pyridine / CH₂Cl₂

3: 96 percent / NaOMe / methanol

4: 47 percent / lipase PS (Pseudomonas cepacia) / various solvent(s) / 24 h / 20 °C

5: 87 percent / NaOMe / methanol

6: 64 percent / H₂ / PtO₂ / acetic acid

7: pyridine / CH₂Cl₂

8: dimethylformamide / Heating

With pyridine; sodium tetrahydroborate; Lipase PS (Pseudomonas cepacia); hydrogen; sodium methylate; platinum(IV) oxide; In methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; 1: Hydrogenation / 2: Acylation / 3: Hydrolysis / 4: Acetylation / 5: Deacetylation / 6: Catalytic hydrogenation / 7: Tosylation / 8: Acetylation;
DOI:10.1002/(SICI)1522-2675(19991006)82:10<1762::AID-HLCA1762>3.0.CO;2-1