(Z)-3-(2,4-Dimethyl-phenyl)-2-(1-methyl-1H-imidazo[4,5-b]pyridin-2-yl)-thioacrylamide

Base Information

Chemical Name:(Z)-3-(2,4-Dimethyl-phenyl)-2-(1-methyl-1H-imidazo[4,5-b]pyridin-2-yl)-thioacrylamide
CAS No.:137242-51-4
Molecular Formula:C₁₈H₁₈N₄S
Molecular Weight:322.434
Hs Code.:

Synonyms:(Z)-3-(2,4-Dimethyl-phenyl)-2-(1-methyl-1H-imidazo[4,5-b]pyridin-2-yl)-thioacrylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-(2,4-Dimethyl-phenyl)-2-(1-methyl-1H-imidazo[4,5-b]pyridin-2-yl)-thioacrylamide

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Technology Process of (Z)-3-(2,4-Dimethyl-phenyl)-2-(1-methyl-1H-imidazo[4,5-b]pyridin-2-yl)-thioacrylamide

There total 3 articles about (Z)-3-(2,4-Dimethyl-phenyl)-2-(1-methyl-1H-imidazo[4,5-b]pyridin-2-yl)-thioacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 137242-48-9
(E)-3-(2,4-Dimethyl-phenyl)-2-(1-methyl-1H-imidazo[4,5-b]pyridin-2-yl)-acrylonitrile

: 137242-51-4
(Z)-3-(2,4-Dimethyl-phenyl)-2-(1-methyl-1H-imidazo[4,5-b]pyridin-2-yl)-thioacrylamide

Guidance literature:: With hydrogen sulfide; triethylamine; In pyridine; for 72h; Ambient temperature;
DOI:10.1002/ardp.2503240903

Reference yield:

: 133466-04-3
1-methyl-1H-2-cyanomethyl-imidazo<4,5-b>pyridine

: 137242-51-4
(Z)-3-(2,4-Dimethyl-phenyl)-2-(1-methyl-1H-imidazo[4,5-b]pyridin-2-yl)-thioacrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / piperidine / ethanol / 2 h / Heating

2: 58 percent / H₂S, N(C₂H₅)3 / pyridine / 72 h / Ambient temperature

With piperidine; hydrogen sulfide; triethylamine; In pyridine; ethanol;
DOI:10.1002/ardp.2503240903

Reference yield:

: 15764-16-6
2,4-dimethylbenzaldehyde

: 137242-51-4
(Z)-3-(2,4-Dimethyl-phenyl)-2-(1-methyl-1H-imidazo[4,5-b]pyridin-2-yl)-thioacrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / piperidine / ethanol / 2 h / Heating

2: 58 percent / H₂S, N(C₂H₅)3 / pyridine / 72 h / Ambient temperature

With piperidine; hydrogen sulfide; triethylamine; In pyridine; ethanol;
DOI:10.1002/ardp.2503240903