allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-6-(phenylseleno)hexanoate

Base Information

Chemical Name:allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-6-(phenylseleno)hexanoate
CAS No.:113599-72-7
Molecular Formula:C₃₈H₃₈N₂O₅Se
Molecular Weight:681.69
Hs Code.:

Synonyms:allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-6-(phenylseleno)hexanoate

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Chemical Property of allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-6-(phenylseleno)hexanoate

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Technology Process of allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-6-(phenylseleno)hexanoate

There total 7 articles about allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-6-(phenylseleno)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 113599-65-8
allyl 2-<(3S,4S)-4-<<(tert-butyldimethylsilyl)oxy>methyl>-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-6-(phenylseleno)hexanoate

: 113599-72-7
allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-6-(phenylseleno)hexanoate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1021/jm00401a020

Reference yield:

: 40630-84-0
allyl bromoacetate

: 113599-72-7
allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-6-(phenylseleno)hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / tetrabutylammonium bromide, KOH / tetrahydrofuran / 20 h

2: 76 percent / lithium bis(trimethylsilyl)amide / tetrahydrofuran / -78 °C

3: 73 percent / tetrabutylammonium fluoride / tetrahydrofuran

With potassium hydroxide; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1021/jm00401a020

Reference yield:

: 23768-06-1
4-(phenylseleno)butanoic acid

: 113599-72-7
allyl 2-<(3S,4S)-4-(hydroxymethyl)-2-oxo-3-tritylamino-1-azetidinyl>-3-oxo-6-(phenylseleno)hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / oxalyl chloride / 16 h / Ambient temperature

2: 76 percent / lithium bis(trimethylsilyl)amide / tetrahydrofuran / -78 °C

3: 73 percent / tetrabutylammonium fluoride / tetrahydrofuran

With oxalyl dichloride; tetrabutyl ammonium fluoride; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1021/jm00401a020