2,5-dibromo-9,9'-bis(4-(bis(2-acetoxyethyl)amino)phenyl)fluorene

Base Information

• Chemical Name: 2,5-dibromo-9,9'-bis(4-(bis(2-acetoxyethyl)amino)phenyl)fluorene
• CAS No.: 1106670-18-1
• Molecular Formula: C₄₁H₄₂Br₂N₂O₈
• Molecular Weight: 850.601
• Mol file: 1106670-18-1.mol

Synonyms:2,5-dibromo-9,9'-bis(4-(bis(2-acetoxyethyl)amino)phenyl)fluorene

Chemical Property of 2,5-dibromo-9,9'-bis(4-(bis(2-acetoxyethyl)amino)phenyl)fluorene

Chemical Property:

Purity/Quality:

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Technology Process of 2,5-dibromo-9,9'-bis(4-(bis(2-acetoxyethyl)amino)phenyl)fluorene

There total 1 articles about 2,5-dibromo-9,9'-bis(4-(bis(2-acetoxyethyl)amino)phenyl)fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2,7-dibromofluorene-9-one (14348-75-5) + bis(2-acetoxyethyl)aniline (19249-34-4) → 2,5-dibromo-9,9'-bis(4-(bis(2-acetoxyethyl)amino)phenyl)fluorene (1106670-18-1)

Guidance literature:

With methanesulfonic acid; In tetrachloromethane; at 80 ℃; for 40h;

DOI:10.1039/b815431g

Reference yield: 67.0%

2,5-dibromo-9,9'-bis(4-(bis(2-acetoxyethyl)amino)phenyl)fluorene (1106670-18-1) + 9,9-dihexylfluorene-2-boronic acid (371193-08-7) → TFE (1106670-19-2)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 75 ℃; for 24h;

DOI:10.1039/b815431g

upstream raw materials:

2,7-dibromofluorene-9-one

bis(2-acetoxyethyl)aniline

Downstream raw materials:

TFE