C₄₅H₅₈O₁₀Si

Base Information

Chemical Name:C₄₅H₅₈O₁₀Si
CAS No.:1315567-81-7
Molecular Formula:C₄₅H₅₈O₁₀Si
Molecular Weight:787.035
Hs Code.:

C<sub>45</sub>H<sub>58</sub>O<sub>10</sub>Si

Synonyms:C₄₅H₅₈O₁₀Si

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Chemical Property of C₄₅H₅₈O₁₀Si

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Technology Process of C₄₅H₅₈O₁₀Si

There total 20 articles about C₄₅H₅₈O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1315567-99-7
C₄₃H₅₆O₉Si

: 108-24-7
acetic anhydride

: 1315567-81-7
C₄₅H₅₈O₁₀Si

Guidance literature:: With dmap; In dichloromethane; at 20 ℃;
DOI:10.1038/nchem.1074

Reference yield:

: 1315567-64-6
C₄₄H₄₈O₁₂

: 1315567-81-7
C₄₅H₅₈O₁₀Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / methanol; water / 50 °C

1.2: 0 °C

2.1: 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride / dichloromethane / -78 °C

2.2: 65 °C

3.1: ammonium chloride; zinc / ethanol / 160 °C / Microwave irradiation

4.1: pyridinium p-toluenesulfonate / dichloromethane / 40 °C

5.1: N-Bromosuccinimide; sodium hydrogencarbonate; dibenzoyl peroxide / tetrachloromethane; benzene / 70 °C

5.2: 20 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

7.1: dmap; triethylamine / dichloromethane / 20 °C

8.1: toluene-4-sulfonic acid / methanol; N,N-dimethyl-formamide / 200 °C / Microwave irradiation

9.1: dmap / dichloromethane / 20 °C

With 2,6-dimethylpyridine; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; trifluoromethylsulfonic anhydride; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; ammonium chloride; toluene-4-sulfonic acid; triethylamine; zinc; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene;
DOI:10.1038/nchem.1074

Reference yield:

: C₄₁H₅₅BrO₆Si

: 1315567-81-7
C₄₅H₅₈O₁₀Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: ozone / methanol; dichloromethane / -78 °C

1.2: -78 - 20 °C

2.1: 1H-imidazole; tert-butyldimethylsilyl chloride / dichloromethane / 20 °C

2.2: 20 °C

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 °C

4.1: cerium(III) chloride / tetrahydrofuran / -78 °C

5.1: potassium carbonate / methanol; water / 50 °C

5.2: 0 °C

6.1: 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride / dichloromethane / -78 °C

6.2: 65 °C

7.1: ammonium chloride; zinc / ethanol / 160 °C / Microwave irradiation

8.1: pyridinium p-toluenesulfonate / dichloromethane / 40 °C

9.1: N-Bromosuccinimide; sodium hydrogencarbonate; dibenzoyl peroxide / tetrachloromethane; benzene / 70 °C

9.2: 20 °C

10.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

11.1: dmap; triethylamine / dichloromethane / 20 °C

12.1: toluene-4-sulfonic acid / methanol; N,N-dimethyl-formamide / 200 °C / Microwave irradiation

13.1: dmap / dichloromethane / 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; cerium(III) chloride; trifluoromethylsulfonic anhydride; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; ammonium chloride; Dess-Martin periodane; toluene-4-sulfonic acid; ozone; tert-butyldimethylsilyl chloride; triethylamine; zinc; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene;
DOI:10.1038/nchem.1074