4-Methyl-N-[(3S,4R)-2-oxo-4-((E)-propenyl)-tetrahydro-pyran-3-yl]-benzenesulfonamide

Base Information

Chemical Name:4-Methyl-N-[(3S,4R)-2-oxo-4-((E)-propenyl)-tetrahydro-pyran-3-yl]-benzenesulfonamide
CAS No.:93455-31-3
Molecular Formula:C₁₅H₁₉NO₄S
Molecular Weight:309.386
Hs Code.:

Synonyms:4-Methyl-N-[(3S,4R)-2-oxo-4-((E)-propenyl)-tetrahydro-pyran-3-yl]-benzenesulfonamide

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Chemical Property of 4-Methyl-N-[(3S,4R)-2-oxo-4-((E)-propenyl)-tetrahydro-pyran-3-yl]-benzenesulfonamide

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Technology Process of 4-Methyl-N-[(3S,4R)-2-oxo-4-((E)-propenyl)-tetrahydro-pyran-3-yl]-benzenesulfonamide

There total 10 articles about 4-Methyl-N-[(3S,4R)-2-oxo-4-((E)-propenyl)-tetrahydro-pyran-3-yl]-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 928-97-2
(E)-3-hexen-1-ol

: 93455-31-3
4-Methyl-N-[(3S,4R)-2-oxo-4-((E)-propenyl)-tetrahydro-pyran-3-yl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / pyridine / CH₂Cl₂ / 0.33 h / 0 °C

2: 94 percent / silver nitrate / acetonitrile / 24 h

3: 72 percent / sodium acetate / dimethylsulfoxide / 0.33 h

4: 0.892 g / aluminum chloride / benzene / 24 h / Heating

5: 1,2-dichloro-benzene / 7 h / Heating

With pyridine; sodium acetate; silver nitrate; aluminium trichloride; In dichloromethane; dimethyl sulfoxide; 1,2-dichloro-benzene; acetonitrile; benzene;
DOI:10.1021/jo00200a006

Reference yield:

: 90449-00-6
(E)-3-hexenyl bromoacetate

: 93455-31-3
4-Methyl-N-[(3S,4R)-2-oxo-4-((E)-propenyl)-tetrahydro-pyran-3-yl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / silver nitrate / acetonitrile / 24 h

2: 72 percent / sodium acetate / dimethylsulfoxide / 0.33 h

3: 0.892 g / aluminum chloride / benzene / 24 h / Heating

4: 1,2-dichloro-benzene / 7 h / Heating

With sodium acetate; silver nitrate; aluminium trichloride; In dimethyl sulfoxide; 1,2-dichloro-benzene; acetonitrile; benzene;
DOI:10.1021/jo00200a006

Reference yield:

: 93455-22-2
Nitrooxy-acetic acid (E)-hex-3-enyl ester

: 93455-31-3
4-Methyl-N-[(3S,4R)-2-oxo-4-((E)-propenyl)-tetrahydro-pyran-3-yl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / sodium acetate / dimethylsulfoxide / 0.33 h

2: 0.892 g / aluminum chloride / benzene / 24 h / Heating

3: 1,2-dichloro-benzene / 7 h / Heating

With sodium acetate; aluminium trichloride; In dimethyl sulfoxide; 1,2-dichloro-benzene; benzene;
DOI:10.1021/jo00200a006