3'-(3-chloro-4-nitro-β-styryl)-(2,2':5',2''-terthiophene)

Base Information

• Chemical Name: 3'-(3-chloro-4-nitro-β-styryl)-(2,2':5',2''-terthiophene)
• CAS No.: 1095632-27-1
• Molecular Formula: C₂₀H₁₂ClNO₂S₃
• Molecular Weight: 429.972
• Mol file: 1095632-27-1.mol

Synonyms:3'-(3-chloro-4-nitro-β-styryl)-(2,2':5',2''-terthiophene)

Chemical Property of 3'-(3-chloro-4-nitro-β-styryl)-(2,2':5',2''-terthiophene)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3'-(3-chloro-4-nitro-β-styryl)-(2,2':5',2''-terthiophene)

There total 1 articles about 3'-(3-chloro-4-nitro-β-styryl)-(2,2':5',2''-terthiophene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Chloro-3-chloromethyl-benzene (620-20-2,130468-19-8) + 2,2’:5’,2’’-terthiophene-3’-carboxaldehyde (393109-70-1) → C20H12ClNO2S3 + 3'-(3-chloro-4-nitro-β-styryl)-(2,2':5',2''-terthiophene) (1095632-27-1)

Guidance literature:

1-Chloro-3-chloromethyl-benzene; With sulfuric acid; nitric acid; acetic acid; for 3.5h;

With triphenylphosphine; In benzene; for 3h; Reflux;

2,2’:5’,2’’-terthiophene-3’-carboxaldehyde; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; for 8h; Reflux;

DOI:10.1139/V08-136

Reference yield: 100.0%

3'-(3-chloro-4-nitro-β-styryl)-(2,2':5',2''-terthiophene) (1095632-27-1) → 3'-(3-chloro-4-amino-β-styryl)-(2,2':5',2''-terthiophene) (1095632-31-7)

Guidance literature:

With iron; ammonium chloride; In ethanol; water; at 85 ℃; for 1h;

DOI:10.1139/V08-136

upstream raw materials:

1-Chloro-3-chloromethyl-benzene

2,2’:5’,2’’-terthiophene-3’-carboxaldehyde

Downstream raw materials:

3'-(3-chloro-4-amino-β-styryl)-(2,2':5',2''-terthiophene)