4-ClC₆H₄SbCl₂

Base Information

Chemical Name:4-ClC₆H₄SbCl₂
CAS No.:7277-07-8
Molecular Formula:C₆H₄Cl₃Sb
Molecular Weight:304.207
Hs Code.:

4-ClC<sub>6</sub>H<sub>4</sub>SbCl<sub>2</sub>

Synonyms:4-ClC₆H₄SbCl₂

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Chemical Property of 4-ClC₆H₄SbCl₂

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Technology Process of 4-ClC₆H₄SbCl₂

There total 2 articles about 4-ClC₆H₄SbCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 62170-62-1
(p-chlorophenyl)stibonic acid

: 7277-07-8
4-ClC₆H₄SbCl₂

Guidance literature:: With sulfur dioxide; hydrogen iodide; In ethanol; stibonic acid dissolving in ethanolic HCl; recrystn. from CHCl3 at -60°C;
DOI:10.1021/ja01163a062

Reference yield:

: 7277-07-8
4-ClC₆H₄SbCl₂

Guidance literature:: With hydrogenchloride; tin(ll) chloride;
DOI:10.1021/ja01163a062

Reference yield: 73.0%

: 111-24-0
1,5-dibromo-pentane

: 7277-07-8
4-ClC₆H₄SbCl₂

: 53127-90-5
4-ClC₆H₄SbC₅H₁₀

Guidance literature:: With magnesium; In diethyl ether; Sb compound added to an ether soln. of the Grignard of 1,5-dibromopentane under nitrogen; mixt. refluxed for 1 h; addn. of water; distn. of the ether phase;
DOI:10.1016/S0022-328X(00)89689-8