2-(tert-butyl-diphenyl-silanyloxymethyl)-6-[2-(tert-butyl-diphenyl-silanyloxymethyl)-3,5-dihydroxy-6-(3,4,5,6-tetramethoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3,4,5-triol

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Chemical Name:2-(tert-butyl-diphenyl-silanyloxymethyl)-6-[2-(tert-butyl-diphenyl-silanyloxymethyl)-3,5-dihydroxy-6-(3,4,5,6-tetramethoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3,4,5-triol
CAS No.:870101-19-2
Molecular Formula:C₅₄H₇₆O₁₆Si₂
Molecular Weight:1037.36
Hs Code.:

2-(<i>tert</i>-butyl-diphenyl-silanyloxymethyl)-6-[2-(<i>tert</i>-butyl-diphenyl-silanyloxymethyl)-3,5-dihydroxy-6-(3,4,5,6-tetramethoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3,4,5-triol

Synonyms:2-(tert-butyl-diphenyl-silanyloxymethyl)-6-[2-(tert-butyl-diphenyl-silanyloxymethyl)-3,5-dihydroxy-6-(3,4,5,6-tetramethoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3,4,5-triol

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Chemical Property of 2-(tert-butyl-diphenyl-silanyloxymethyl)-6-[2-(tert-butyl-diphenyl-silanyloxymethyl)-3,5-dihydroxy-6-(3,4,5,6-tetramethoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3,4,5-triol

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Technology Process of 2-(tert-butyl-diphenyl-silanyloxymethyl)-6-[2-(tert-butyl-diphenyl-silanyloxymethyl)-3,5-dihydroxy-6-(3,4,5,6-tetramethoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3,4,5-triol

There total 5 articles about 2-(tert-butyl-diphenyl-silanyloxymethyl)-6-[2-(tert-butyl-diphenyl-silanyloxymethyl)-3,5-dihydroxy-6-(3,4,5,6-tetramethoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3,4,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 870101-18-1
benzoic acid 6-(tert-butyl-diphenyl-silanyloxymethyl)-2-[2-(tert-butyl-diphenyl-silanyloxymethyl)-3,5-dihydroxy-6-(3,4,5,6-tetramethoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-4-yloxy]-4,5-dihydroxy-tetrahydro-pyran-3-yl ester

: 870101-19-2
2-(tert-butyl-diphenyl-silanyloxymethyl)-6-[2-(tert-butyl-diphenyl-silanyloxymethyl)-3,5-dihydroxy-6-(3,4,5,6-tetramethoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3,4,5-triol

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1039/b507468a

Reference yield:

: 870101-10-3
2-(tert-butyl-diphenyl-silanyloxymethyl)-6-(3,4,5,6-tetramethoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-3,4,5-triol

: 870101-19-2
2-(tert-butyl-diphenyl-silanyloxymethyl)-6-[2-(tert-butyl-diphenyl-silanyloxymethyl)-3,5-dihydroxy-6-(3,4,5,6-tetramethoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / NBS; BF₃*Et₂O

2: 60 percent / NaOMe / methanol

With N-Bromosuccinimide; boron trifluoride diethyl etherate; sodium methylate; In methanol;
DOI:10.1039/b507468a

Reference yield:

: 870101-08-9
benzoic acid 6-(tert-butyl-diphenyl-silanyloxymethyl)-4,5-dihydroxy-2-(3,4,5,6-tetramethoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-3-yl ester

: 870101-19-2
2-(tert-butyl-diphenyl-silanyloxymethyl)-6-[2-(tert-butyl-diphenyl-silanyloxymethyl)-3,5-dihydroxy-6-(3,4,5,6-tetramethoxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-4-yloxy]-tetrahydro-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / NaOMe

2: 50 percent / NBS; BF₃*Et₂O

3: 60 percent / NaOMe / methanol

With N-Bromosuccinimide; boron trifluoride diethyl etherate; sodium methylate; In methanol;
DOI:10.1039/b507468a