methyl 2-(((tert-butoxycarbonyl)oxy)(3,4-dichlorophenyl)methyl)acrylate

Base Information

Chemical Name:methyl 2-(((tert-butoxycarbonyl)oxy)(3,4-dichlorophenyl)methyl)acrylate
CAS No.:1132641-33-8
Molecular Formula:C₁₆H₁₈Cl₂O₅
Molecular Weight:361.222
Hs Code.:

Synonyms:methyl 2-(((tert-butoxycarbonyl)oxy)(3,4-dichlorophenyl)methyl)acrylate

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Chemical Property of methyl 2-(((tert-butoxycarbonyl)oxy)(3,4-dichlorophenyl)methyl)acrylate

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Technology Process of methyl 2-(((tert-butoxycarbonyl)oxy)(3,4-dichlorophenyl)methyl)acrylate

There total 1 articles about methyl 2-(((tert-butoxycarbonyl)oxy)(3,4-dichlorophenyl)methyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methyl 2-[(3,4-dichlorophenyl)(hydroxy)methyl]prop-2-enoate

: 24424-99-5
di-tert-butyl dicarbonate

: 1132641-33-8
methyl 2-(((tert-butoxycarbonyl)oxy)(3,4-dichlorophenyl)methyl)acrylate

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c9cc04542b

Reference yield: 99.0%

: 1132641-33-8
methyl 2-(((tert-butoxycarbonyl)oxy)(3,4-dichlorophenyl)methyl)acrylate

: N-acetyl-1-(4'-chlorophenyl)-propenamine

: C₂₂H₂₀Cl₃NO₃

Guidance literature:: With hydroquinidine (anthraquinone-1,4-diyl) diether; In toluene; at 50 ℃; for 96h; optical yield given as %ee; enantioselective reaction;
DOI:10.1039/c0cc05616b

Reference yield: 99.0%

: 1132641-33-8
methyl 2-(((tert-butoxycarbonyl)oxy)(3,4-dichlorophenyl)methyl)acrylate

: 497235-37-7
6-chloro-1-[(4-methoxyphenyl)methyl]-4-(trifluoromethyl)hydroquinazolin-2-one

: methyl 9-chloro-1-(3,4-dichlorophenyl)-6-(4-methoxybenzyl)-5-oxo-10b-(trifluoromethyl)-1,5,6,10b-tetrahydropyrrolo[1,2-c]quinazoline-2-carboxylate

Guidance literature:: With tributylphosphine; In toluene; at 20 ℃; for 3h; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201300342