(2S,3R,4S,5S,6S)-2-(4-((4-(difluoromethyl)phenylcarbamoyloxy)methyl)phenoxy)-6-(methoxycarbonyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Base Information

Chemical Name:(2S,3R,4S,5S,6S)-2-(4-((4-(difluoromethyl)phenylcarbamoyloxy)methyl)phenoxy)-6-(methoxycarbonyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate
CAS No.:1373332-71-8
Molecular Formula:C₂₈H₂₉F₂NO₁₂
Molecular Weight:609.535
Hs Code.:

Synonyms:(2S,3R,4S,5S,6S)-2-(4-((4-(difluoromethyl)phenylcarbamoyloxy)methyl)phenoxy)-6-(methoxycarbonyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Chemical Property of (2S,3R,4S,5S,6S)-2-(4-((4-(difluoromethyl)phenylcarbamoyloxy)methyl)phenoxy)-6-(methoxycarbonyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Technology Process of (2S,3R,4S,5S,6S)-2-(4-((4-(difluoromethyl)phenylcarbamoyloxy)methyl)phenoxy)-6-(methoxycarbonyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

There total 9 articles about (2S,3R,4S,5S,6S)-2-(4-((4-(difluoromethyl)phenylcarbamoyloxy)methyl)phenoxy)-6-(methoxycarbonyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1373332-71-8
(2S,3R,4S,5S,6S)-2-(4-((4-(difluoromethyl)phenylcarbamoyloxy)methyl)phenoxy)-6-(methoxycarbonyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: Multi-step reaction with 3 steps

1: silver(l) oxide / acetonitrile / 18 h / 23 °C / Darkness

2: sodium tetrahydroborate / methanol; dichloromethane / 0 °C

3: dichloromethane; toluene / 20 - 80 °C

With sodium tetrahydroborate; silver(l) oxide; In methanol; dichloromethane; toluene; acetonitrile;
DOI:10.1002/anie.201107787

Reference yield:

: 1571-08-0
methyl 4-formylbenzoate

: 1373332-71-8
(2S,3R,4S,5S,6S)-2-(4-((4-(difluoromethyl)phenylcarbamoyloxy)methyl)phenoxy)-6-(methoxycarbonyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: Multi-step reaction with 6 steps

1: diethylamino-sulfur trifluoride / 24 h / 23 °C

2: lithium hydroxide monohydrate / tetrahydrofuran; methanol / 0 °C

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C

4: sodium azide / water; acetone / 0 °C

5: toluene / 1.5 h / 110 °C

6: dichloromethane; toluene / 20 - 80 °C

With sodium azide; oxalyl dichloride; lithium hydroxide monohydrate; diethylamino-sulfur trifluoride; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; dichloromethane; water; acetone; toluene;
DOI:10.1002/anie.201107787

Reference yield:

: 4-(difluoromethyl)benzoyl chloride

: 1373332-71-8
(2S,3R,4S,5S,6S)-2-(4-((4-(difluoromethyl)phenylcarbamoyloxy)methyl)phenoxy)-6-(methoxycarbonyl)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / water; acetone / 0 °C

2: toluene / 1.5 h / 110 °C

3: dichloromethane; toluene / 20 - 80 °C

With sodium azide; In dichloromethane; water; acetone; toluene;
DOI:10.1002/anie.201107787