3-(5-(5-(4-(bis(7-(hexyloxy)-9,9-dimethyl-9H-fluoren-2-yl)amino)phenyl)thiophen-2-yl)-1-methyl-1H-pyrrol-2-yl)-4-hydroxycyclobut-3-ene-1,2-dione

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Chemical Name:3-(5-(5-(4-(bis(7-(hexyloxy)-9,9-dimethyl-9H-fluoren-2-yl)amino)phenyl)thiophen-2-yl)-1-methyl-1H-pyrrol-2-yl)-4-hydroxycyclobut-3-ene-1,2-dione
CAS No.:1289537-27-4
Molecular Formula:C₆₁H₆₂N₂O₅S
Molecular Weight:935.24
Hs Code.:

Synonyms:3-(5-(5-(4-(bis(7-(hexyloxy)-9,9-dimethyl-9H-fluoren-2-yl)amino)phenyl)thiophen-2-yl)-1-methyl-1H-pyrrol-2-yl)-4-hydroxycyclobut-3-ene-1,2-dione

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Chemical Property of 3-(5-(5-(4-(bis(7-(hexyloxy)-9,9-dimethyl-9H-fluoren-2-yl)amino)phenyl)thiophen-2-yl)-1-methyl-1H-pyrrol-2-yl)-4-hydroxycyclobut-3-ene-1,2-dione

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Technology Process of 3-(5-(5-(4-(bis(7-(hexyloxy)-9,9-dimethyl-9H-fluoren-2-yl)amino)phenyl)thiophen-2-yl)-1-methyl-1H-pyrrol-2-yl)-4-hydroxycyclobut-3-ene-1,2-dione

There total 3 articles about 3-(5-(5-(4-(bis(7-(hexyloxy)-9,9-dimethyl-9H-fluoren-2-yl)amino)phenyl)thiophen-2-yl)-1-methyl-1H-pyrrol-2-yl)-4-hydroxycyclobut-3-ene-1,2-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₁H₆₁ClN₂O₄S

: 1289537-27-4
3-(5-(5-(4-(bis(7-(hexyloxy)-9,9-dimethyl-9H-fluoren-2-yl)amino)phenyl)thiophen-2-yl)-1-methyl-1H-pyrrol-2-yl)-4-hydroxycyclobut-3-ene-1,2-dione

Guidance literature:: With triethylamine; In acetone; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1039/c0cc05378c

Reference yield:

: 1289537-24-1
7-(hexyloxy)-N-(7-(hexyloxy)-9,9-dimethyl-9H-fluoren-2-yl)-9,9-dimethyl-N-(4-(5-(1-methyl-1H-pyrrol-2-yl)thiophen-2-yl)phenyl)-9H-fluoren-2-amine

: 1289537-27-4
3-(5-(5-(4-(bis(7-(hexyloxy)-9,9-dimethyl-9H-fluoren-2-yl)amino)phenyl)thiophen-2-yl)-1-methyl-1H-pyrrol-2-yl)-4-hydroxycyclobut-3-ene-1,2-dione

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 1 h / 20 °C / Inert atmosphere

2: triethylamine / acetone / 6 h / 20 °C / Inert atmosphere

With triethylamine; In diethyl ether; acetone;
DOI:10.1039/c0cc05378c

Reference yield:

: 1289537-19-4
N-(4-(5-bromothiophen-2-yl)phenyl)-7-(hexyloxy)-N-(7-(hexyloxy)-9,9-dimethyl-9H-fluoren-2-yl)-9,9-dimethyl-9H-fluoren-2-amine

: 1289537-27-4
3-(5-(5-(4-(bis(7-(hexyloxy)-9,9-dimethyl-9H-fluoren-2-yl)amino)phenyl)thiophen-2-yl)-1-methyl-1H-pyrrol-2-yl)-4-hydroxycyclobut-3-ene-1,2-dione

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 48 h / Inert atmosphere; Reflux

2: diethyl ether / 1 h / 20 °C / Inert atmosphere

3: triethylamine / acetone / 6 h / 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In diethyl ether; acetone; toluene; 1: Stille coupling;
DOI:10.1039/c0cc05378c