tert-Butyl-diphenyl-(2-phenylselanylmethyl-6-vinyl-[1,3]dioxan-4-ylmethoxy)-silane

Base Information

Chemical Name:tert-Butyl-diphenyl-(2-phenylselanylmethyl-6-vinyl-[1,3]dioxan-4-ylmethoxy)-silane
CAS No.:104085-36-1
Molecular Formula:C₃₀H₃₆O₃SeSi
Molecular Weight:551.66
Hs Code.:

Synonyms:tert-Butyl-diphenyl-(2-phenylselanylmethyl-6-vinyl-[1,3]dioxan-4-ylmethoxy)-silane

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Chemical Property of tert-Butyl-diphenyl-(2-phenylselanylmethyl-6-vinyl-[1,3]dioxan-4-ylmethoxy)-silane

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Technology Process of tert-Butyl-diphenyl-(2-phenylselanylmethyl-6-vinyl-[1,3]dioxan-4-ylmethoxy)-silane

There total 4 articles about tert-Butyl-diphenyl-(2-phenylselanylmethyl-6-vinyl-[1,3]dioxan-4-ylmethoxy)-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 71338-47-1
2-phenylselenoacetaldehyde diethylacetal

: 1-(tert-Butyl-diphenyl-silanyloxy)-hex-5-ene-2,4-diol

: 104085-36-1
tert-Butyl-diphenyl-(2-phenylselanylmethyl-6-vinyl-[1,3]dioxan-4-ylmethoxy)-silane

Guidance literature:: With Amberlite IR 120; In toluene; Heating;
DOI:10.1039/c39860000325

Reference yield:

: 34837-55-3
Phenylselenyl bromide

: 104085-36-1
tert-Butyl-diphenyl-(2-phenylselanylmethyl-6-vinyl-[1,3]dioxan-4-ylmethoxy)-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) di-isopropylamine

2: 87 percent / Amberlite IR 120 / toluene / Heating

With Amberlite IR 120; diisopropylamine; In toluene;
DOI:10.1039/c39860000325

Reference yield:

: 253880-23-8
Hex-5-ene-1,2,4-triol

: 104085-36-1
tert-Butyl-diphenyl-(2-phenylselanylmethyl-6-vinyl-[1,3]dioxan-4-ylmethoxy)-silane

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole

2: 87 percent / Amberlite IR 120 / toluene / Heating

With 1H-imidazole; Amberlite IR 120; In toluene;
DOI:10.1039/c39860000325