C₂₆H₃₈O₇

Base Information

Chemical Name:C₂₆H₃₈O₇
CAS No.:902454-72-2
Molecular Formula:C₂₆H₃₈O₇
Molecular Weight:462.584
Hs Code.:

C<sub>26</sub>H<sub>38</sub>O<sub>7</sub>

Synonyms:C₂₆H₃₈O₇

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Chemical Property of C₂₆H₃₈O₇

Chemical Property:

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Technology Process of C₂₆H₃₈O₇

There total 25 articles about C₂₆H₃₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 902454-67-5
C₃₈H₆₆O₇Si₂

: 902454-72-2
C₂₆H₃₈O₇

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 25 ℃; for 16h;
DOI:10.1039/b602021f

Reference yield:

: 902454-48-2
C₁₀H₂₀O₃

: 902454-72-2
C₂₆H₃₈O₇

Guidance literature:: Multi-step reaction with 15 steps

1.1: NaH / tetrahydrofuran; various solvent(s) / 0.5 h / 0 °C

2.1: O₃ / CH₂Cl₂ / -78 °C

2.2: PPh₃ / CH₂Cl₂ / 1 h / -78 - 25 °C

3.1: 28.9 g / benzene / 40 h / 70 °C

4.1: 96 percent / DIBAL-H / toluene; tetrahydrofuran / 2.5 h / -78 °C

5.1: TsOH*H₂O / acetone / 3 h / 25 °C

6.1: 25.84 g / imidazole; 4-DMAP / CH₂Cl₂ / 1.5 h / 25 °C

7.1: 78 percent / NaH₂PO₄; NaClO₂; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 2 h / 25 °C

8.1: 97 percent / K₂CO₃ / acetone / 16 h / 25 °C

9.1: KHMDS / tetrahydrofuran; toluene / 0.5 h / -78 °C

9.2: Davis oxaziridine / tetrahydrofuran; toluene / 1 h / -78 °C

10.1: 86 percent / imidazole; 4-DMAP / CH₂Cl₂ / 16 h / 25 °C

11.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

11.2: 92 percent / tetrahydrofuran; hexane / 1 h / -78 °C

12.1: LiCl / acetonitrile / 0.17 h / 25 °C

12.2: i-Pr₂NEt / acetonitrile / 0.17 h / 25 °C

12.3: 97 percent / acetonitrile / 36 h / 25 °C

13.1: KHMDS / tetrahydrofuran; toluene / 0.5 h / 25 °C

13.2: 94 percent / tetrahydrofuran; toluene / -78 - 25 °C

14.1: 87 percent / PPTS / ethanol / 20 h / 45 °C

15.1: 79 percent / TsOH*H₂O / methanol / 16 h / 25 °C

With 1H-imidazole; dmap; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; pyridinium p-toluenesulfonate; potassium hexamethylsilazane; sodium hydride; diisobutylaluminium hydride; potassium carbonate; toluene-4-sulfonic acid; ozone; lithium chloride; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; acetone; toluene; acetonitrile; tert-butyl alcohol; benzene; 3.1: Wittig reaction / 12.1: Horner-Wadsworth-Emmons olefination / 13.2: Wittig methylenation;
DOI:10.1039/b602021f

Reference yield:

: 902454-45-9
C₁₂H₂₄O₄Si

: 902454-72-2
C₂₆H₃₈O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: LiCl / acetonitrile / 0.17 h / 25 °C

1.2: i-Pr₂NEt / acetonitrile / 0.17 h / 25 °C

1.3: acetonitrile / 48 h / 25 °C

2.1: KHMDS / tetrahydrofuran; toluene / 0.5 h / 25 °C

2.2: 94 percent / tetrahydrofuran; toluene / -78 - 25 °C

3.1: 87 percent / PPTS / ethanol / 20 h / 45 °C

4.1: 79 percent / TsOH*H₂O / methanol / 16 h / 25 °C

With pyridinium p-toluenesulfonate; potassium hexamethylsilazane; toluene-4-sulfonic acid; lithium chloride; In tetrahydrofuran; methanol; ethanol; toluene; acetonitrile; 1.1: Horner-Wadsworth-Emmons olefination / 2.2: Wittig methylenation;
DOI:10.1039/b602021f