N-((1S,2S)-2-(2-cyclohexyloxy)-1-indanyl)-N′-(2,3,4,5,6-pentamethylphenyl)oxalamide

Base Information

Chemical Name:N-((1S,2S)-2-(2-cyclohexyloxy)-1-indanyl)-N′-(2,3,4,5,6-pentamethylphenyl)oxalamide
CAS No.:1579250-36-4
Molecular Formula:C₂₈H₃₆N₂O₃
Molecular Weight:448.605
Hs Code.:

Synonyms:N-((1S,2S)-2-(2-cyclohexyloxy)-1-indanyl)-N′-(2,3,4,5,6-pentamethylphenyl)oxalamide

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Chemical Property of N-((1S,2S)-2-(2-cyclohexyloxy)-1-indanyl)-N′-(2,3,4,5,6-pentamethylphenyl)oxalamide

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Technology Process of N-((1S,2S)-2-(2-cyclohexyloxy)-1-indanyl)-N′-(2,3,4,5,6-pentamethylphenyl)oxalamide

There total 4 articles about N-((1S,2S)-2-(2-cyclohexyloxy)-1-indanyl)-N′-(2,3,4,5,6-pentamethylphenyl)oxalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: N-((1S,2S)-2-(2-cyclohexen-1-yloxy)-1-indanyl)-N′-(2,3,4,5,6-pentamethylphenyl)oxalamide

: 1579250-36-4
N-((1S,2S)-2-(2-cyclohexyloxy)-1-indanyl)-N′-(2,3,4,5,6-pentamethylphenyl)oxalamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 12h;
DOI:10.1021/jo500068p

Reference yield:

: 2243-30-3,738542-25-1
pentamethylaniline

: 1579250-36-4
N-((1S,2S)-2-(2-cyclohexyloxy)-1-indanyl)-N′-(2,3,4,5,6-pentamethylphenyl)oxalamide

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dichloromethane / 18 h / 0 - 20 °C

2: dichloromethane / 60 h / Reflux

3: silver(l) oxide / 1,2-dichloro-ethane / 48 h / 80 °C

4: palladium 10% on activated carbon; hydrogen / ethanol / 12 h / 20 °C

With pyridine; palladium 10% on activated carbon; hydrogen; silver(l) oxide; In ethanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jo500068p

Reference yield:

: 1579250-33-1
N-(2,3,4,5,6-pentamethylphenyl)-N′-((1S,2S)-2-hydroxy-1-indanyl)oxalamide

: 1579250-36-4
N-((1S,2S)-2-(2-cyclohexyloxy)-1-indanyl)-N′-(2,3,4,5,6-pentamethylphenyl)oxalamide

Guidance literature:: Multi-step reaction with 2 steps

1: silver(l) oxide / 1,2-dichloro-ethane / 48 h / 80 °C

2: palladium 10% on activated carbon; hydrogen / ethanol / 12 h / 20 °C

With palladium 10% on activated carbon; hydrogen; silver(l) oxide; In ethanol; 1,2-dichloro-ethane;
DOI:10.1021/jo500068p