(R)-7-acetoxy-2-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine

Base Information

Chemical Name:(R)-7-acetoxy-2-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine
CAS No.:1204581-64-5
Molecular Formula:C₁₆H₁₅NO₂
Molecular Weight:253.301
Hs Code.:

Synonyms:(R)-7-acetoxy-2-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-7-acetoxy-2-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine

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Technology Process of (R)-7-acetoxy-2-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine

There total 2 articles about (R)-7-acetoxy-2-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 85-44-9
phthalic anhydride

: 108-05-4,9003-20-7
vinyl acetate

: 97360-42-4
7-hydroxy-2-phenyl-6,7-dihydro-5H-<1>pyridine

: 1204581-64-5
(R)-7-acetoxy-2-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine

: 1204581-66-7
2-{[(S)-2-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridin-7-yloxy]carbonyl}benzoic acid

Guidance literature:: vinyl acetate; 7-hydroxy-2-phenyl-6,7-dihydro-5H-<1>pyridine; In di-isopropyl ether; at 60 ℃; for 30h; Inert atmosphere; Enzymatic reaction;

phthalic anhydride; With triethylamine; In dichloromethane; for 6h; optical yield given as %ee; enantioselective reaction; Reflux; Inert atmosphere;
DOI:10.1055/s-0029-1216997

Reference yield:

: 108-05-4,9003-20-7
vinyl acetate

: 97360-42-4
7-hydroxy-2-phenyl-6,7-dihydro-5H-<1>pyridine

: 1204581-64-5
(R)-7-acetoxy-2-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine

: 247185-53-1
(S)-7-hydroxy-2-phenyl-6,7-dihydro-5H-<1>pyridine

Guidance literature:: With Candida antarctica lipase B immobilized on acrylic resin; In di-isopropyl ether; at 60 ℃; for 30h; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Enzymatic reaction;
DOI:10.1055/s-0029-1216997