N-hydroxy-4-((1-(4-hydroxyphenethyl)-3-(2-methoxyphenyl)ureido)methyl)-benzamide

Base Information

Chemical Name:N-hydroxy-4-((1-(4-hydroxyphenethyl)-3-(2-methoxyphenyl)ureido)methyl)-benzamide
CAS No.:1403690-30-1
Molecular Formula:C₂₄H₂₅N₃O₅
Molecular Weight:435.48
Hs Code.:

Synonyms:N-hydroxy-4-((1-(4-hydroxyphenethyl)-3-(2-methoxyphenyl)ureido)methyl)-benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-hydroxy-4-((1-(4-hydroxyphenethyl)-3-(2-methoxyphenyl)ureido)methyl)-benzamide

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Technology Process of N-hydroxy-4-((1-(4-hydroxyphenethyl)-3-(2-methoxyphenyl)ureido)methyl)-benzamide

There total 4 articles about N-hydroxy-4-((1-(4-hydroxyphenethyl)-3-(2-methoxyphenyl)ureido)methyl)-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1403690-23-2
methyl 4-((1-(4-hydroxyphenethyl)-3-(2-methoxyphenyl)ureido)methyl)-benzoate

: 1403690-30-1
N-hydroxy-4-((1-(4-hydroxyphenethyl)-3-(2-methoxyphenyl)ureido)methyl)-benzamide

Guidance literature:: With hydroxylamine; sodium hydroxide; In tetrahydrofuran; methanol; water; at 0 - 20 ℃; for 0.5h;
DOI:10.1021/jm301098e

Reference yield: 63.0%

: 1403690-30-1
N-hydroxy-4-((1-(4-hydroxyphenethyl)-3-(2-methoxyphenyl)ureido)methyl)-benzamide

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; water; at 0 - 20 ℃; for 0.5h;

Reference yield:

: 51-67-2
tyrosamine

: 1403690-30-1
N-hydroxy-4-((1-(4-hydroxyphenethyl)-3-(2-methoxyphenyl)ureido)methyl)-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium cyanoborohydride; acetic acid / dichloromethane / 16 h / 20 °C / Inert atmosphere

2: dichloromethane / 16 h / 20 °C / Inert atmosphere

3: sodium hydroxide; hydroxylamine / water; tetrahydrofuran; methanol / 0.5 h / 0 - 20 °C

With hydroxylamine; sodium cyanoborohydride; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/jm301098e