Technology Process of C17H21BrN2O
There total 5 articles about C17H21BrN2O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
5-bromo-2-chloropyridine; C12H19NO*ClH;
With
acetic acid;
at 80 ℃;
for 20h;
With
sodium hydrogencarbonate;
In
water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 1.5 h
2: hydrogenchloride; hydrogen / palladium on activated charcoal / methanol; water / 1.5 h / 20 °C
3: acetic acid / 20 h / 80 °C
With
hydrogenchloride; hydrogen; potassium carbonate; acetic acid; potassium iodide;
palladium on activated charcoal;
In
methanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sulfuric acid; water; sodium nitrite / 0 - 5 °C
2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 1.5 h
3: hydrogenchloride; hydrogen / palladium on activated charcoal / methanol; water / 1.5 h / 20 °C
4: acetic acid / 20 h / 80 °C
With
hydrogenchloride; sulfuric acid; water; hydrogen; potassium carbonate; acetic acid; potassium iodide; sodium nitrite;
palladium on activated charcoal;
In
methanol; water; N,N-dimethyl-formamide;