(η5-C5Me5)(PMe3)2Ru(CCPh)

Base Information

• Chemical Name: (η5-C5Me5)(PMe3)2Ru(CCPh)
• CAS No.: 106734-53-6
• Molecular Formula: C₂₄H₃₈P₂Ru
• Molecular Weight: 489.583

Synonyms:(η5-C5Me5)(PMe3)2Ru(CCPh)

Chemical Property of (η5-C5Me5)(PMe3)2Ru(CCPh)

Chemical Property:

Purity/Quality:

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Technology Process of (η5-C5Me5)(PMe3)2Ru(CCPh)

There total 1 articles about (η5-C5Me5)(PMe3)2Ru(CCPh) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(η5-C5Me5)Ru(PMe3)2(OH) + phenylacetylene (536-74-3) → (η5-C5Me5)(PMe3)2Ru(CCPh) (106734-53-6)

Guidance literature:

In tetrahydrofuran; react. in a vac. dry box; addn. of HCCPh to a soln. of Ru-complex in THF at -40°C, warming to room temp., stirring for 12 h; evapn.(vac.), slurrying with petroleum ether and THF, filtration, evapn. of soln., slow cooling to -78°C, filtration, second crop by evapn. of supernatant; elem. anal.;

DOI:10.1021/ja00239a026

Reference yield:

(η5-C5Me5)(PMe3)2Ru(CCPh) (106734-53-6) → (η5-C5Me5)(PMe3)Ru(CCPh) + trimethylphosphane (594-09-2)

Guidance literature:

With P(CD₃)3; In benzene-d6; exclusion of air and moisture; NMR-tube charged with Ru-compd., solvent added, P(CD3)3 added; not isolated, monitored by H-NMR spectroscopy; Kinetics;

upstream raw materials:

phenylacetylene

Downstream raw materials:

trimethylphosphane

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