N-[4-(1-benzenesulfonyl-1H-indol-2-yl)but-1-enyl]-N-benzyl-2-ethylsulfinylacetamide

Base Information

Chemical Name:N-[4-(1-benzenesulfonyl-1H-indol-2-yl)but-1-enyl]-N-benzyl-2-ethylsulfinylacetamide
CAS No.:459831-90-4
Molecular Formula:C₂₉H₃₀N₂O₄S₂
Molecular Weight:534.7
Hs Code.:

Synonyms:N-[4-(1-benzenesulfonyl-1H-indol-2-yl)but-1-enyl]-N-benzyl-2-ethylsulfinylacetamide

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Chemical Property of N-[4-(1-benzenesulfonyl-1H-indol-2-yl)but-1-enyl]-N-benzyl-2-ethylsulfinylacetamide

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Technology Process of N-[4-(1-benzenesulfonyl-1H-indol-2-yl)but-1-enyl]-N-benzyl-2-ethylsulfinylacetamide

There total 4 articles about N-[4-(1-benzenesulfonyl-1H-indol-2-yl)but-1-enyl]-N-benzyl-2-ethylsulfinylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 459832-04-3
N-[4-(1-benzenesulfonyl-1H-indol-2-yl)but-1-enyl]-N-benzyl-2-ethylsulfenylacetamide

: 459831-90-4
N-[4-(1-benzenesulfonyl-1H-indol-2-yl)but-1-enyl]-N-benzyl-2-ethylsulfinylacetamide

Guidance literature:: With sodium periodate; In 1,4-dioxane; water; at 20 ℃; for 12h;
DOI:10.1021/jo020083x

Reference yield:

: 165532-83-2
1-Benzenesulfonyl-2-(4-bromobutanyl)-1H-indole

: 459831-90-4
N-[4-(1-benzenesulfonyl-1H-indol-2-yl)but-1-enyl]-N-benzyl-2-ethylsulfinylacetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / silver(I) tetrafluoroborate; DMSO / 18 h / 20 °C

2: magnesium sulfate / CH₂Cl₂ / 2 h / 20 °C

3: 0.9 g / pyridine / CH₂Cl₂ / 3 h / 20 °C

4: 68 percent / sodium periodate / dioxane; H₂O / 12 h / 20 °C

With pyridine; sodium periodate; silver tetrafluoroborate; magnesium sulfate; dimethyl sulfoxide; In 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo020083x

Reference yield:

: 459832-03-2
4-(1-benzenesulfonyl-1H-indol-2-yl)butyraldehyde

: 459831-90-4
N-[4-(1-benzenesulfonyl-1H-indol-2-yl)but-1-enyl]-N-benzyl-2-ethylsulfinylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium sulfate / CH₂Cl₂ / 2 h / 20 °C

2: 0.9 g / pyridine / CH₂Cl₂ / 3 h / 20 °C

3: 68 percent / sodium periodate / dioxane; H₂O / 12 h / 20 °C

With pyridine; sodium periodate; magnesium sulfate; In 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo020083x