1-{2-[(4-{[(tert-butoxycarbonyl)(4-hydroxybenzyl)amino]methyl}benzoyl)(methyl)amino]ethyl}piperidin-4-yl biphenyl-2-ylcarbamate

Base Information

• Chemical Name: 1-{2-[(4-{[(tert-butoxycarbonyl)(4-hydroxybenzyl)amino]methyl}benzoyl)(methyl)amino]ethyl}piperidin-4-yl biphenyl-2-ylcarbamate
• CAS No.: 1246248-11-2
• Molecular Formula: C₄₁H₄₈N₄O₆
• Molecular Weight: 692.855

Synonyms:1-{2-[(4-{[(tert-butoxycarbonyl)(4-hydroxybenzyl)amino]methyl}benzoyl)(methyl)amino]ethyl}piperidin-4-yl biphenyl-2-ylcarbamate

Chemical Property of 1-{2-[(4-{[(tert-butoxycarbonyl)(4-hydroxybenzyl)amino]methyl}benzoyl)(methyl)amino]ethyl}piperidin-4-yl biphenyl-2-ylcarbamate

Chemical Property:

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Technology Process of 1-{2-[(4-{[(tert-butoxycarbonyl)(4-hydroxybenzyl)amino]methyl}benzoyl)(methyl)amino]ethyl}piperidin-4-yl biphenyl-2-ylcarbamate

There total 1 articles about 1-{2-[(4-{[(tert-butoxycarbonyl)(4-hydroxybenzyl)amino]methyl}benzoyl)(methyl)amino]ethyl}piperidin-4-yl biphenyl-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1-{2-[(4-{[(tert-butoxycarbonyl)(4-hydroxybenzyl)amino]methyl}benzoyl)(methyl)amino]ethyl}piperidin-4-yl biphenyl-2-ylcarbamate (1246248-11-2)

Guidance literature:

Reference yield: 92.0%

4-[({[(2S)-1'-{2-[(5R)-3-[3,5-Bis(trifluoromethyl)benzoyl]-5-(4-fluorophenyl)-1,3-oxazolidin-5-yl]ethyl}-2,3-dihydrospiro[indene-1,4'-piperidin]-2-yl]oxy}acetyl)(methyl)amino]butanoic acid (1246248-03-2) + 1-{2-[(4-{[(tert-butoxycarbonyl)(4-hydroxybenzyl)amino]methyl}benzoyl)(methyl)amino]ethyl}piperidin-4-yl biphenyl-2-ylcarbamate (1246248-11-2) → 4-{[{4-[(2-{4-[(biphenyl-2-ylcarbamoyl)oxy]piperidin-1-yl}ethyl)(methyl)carbamoyl]benzyl}(tert-butoxycarbonyl)amino]methyl}phenyl 4-[({[(2S)-1'-{2-[(5R)-3-[3,5-bis(trifluoromethyl)benzoyl]-5-(4-fluorophenyl)-1,3-oxazolidin-5-yl]ethyl}-2,3-dihydrospiro[indene-1,4'-piperidin]-2-yl]oxy}acetyl)(methyl)amino]butanoate (1246248-13-4)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

7-[({[(2S)-1'-{2-[(5R)-3-[3,5-Bis(trifluoromethyl)benzoyl]-5-(4-fluorophenyl)-1,3-oxazolidin-5-yl]ethyl}-2,3-dihydrospiro[indene-1,4'-piperidin]-2-yl]oxy}acetyl)(methyl)amino]heptanoic acid (1246248-16-7) + 1-{2-[(4-{[(tert-butoxycarbonyl)(4-hydroxybenzyl)amino]methyl}benzoyl)(methyl)amino]ethyl}piperidin-4-yl biphenyl-2-ylcarbamate (1246248-11-2) → 4-{[{4-[(2-{4-[(biphenyl-2-ylcarbamoyl)oxy]piperidin-1-yl}ethyl)(methyl)carbamoyl]benzyl}(tert-butoxycarbonyl)amino]methyl}phenyl 7-[({[(2S)-1'-{2-[(5R)-3-[3,5-bis(trifluoromethyl)benzoyl]-5-(4-fluorophenyl)-1,3-oxazolidin-5-yl]ethyl}-2,3-dihydrospiro[indene-1,4'-piperidin]-2-yl]oxy}acetyl)(methyl)amino]heptanoate (1246248-17-8)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

Downstream raw materials:

4-{[{4-[(2-{4-[(biphenyl-2-ylcarbamoyl)oxy]piperidin-1-yl}ethyl)(methyl)carbamoyl]benzyl}(tert-butoxycarbonyl)amino]methyl}phenyl 7-[({[(2S)-1'-{2-[(5R)-3-[3,5-bis(trifluoromethyl)benzoyl]-5-(4-fluorophenyl)-1,3-oxazolidin-5-yl]ethyl}-2,3-dihydrospiro[indene-1,4'-piperidin]-2-yl]oxy}acetyl)(methyl)amino]heptanoate

4-{[{4-[(2-{4-[(biphenyl-2-ylcarbamoyl)oxy]piperidin-1-yl}ethyl)(methyl)carbamoyl]benzyl}(tert-butoxycarbonyl)amino]methyl}phenyl 4-[({[(2S)-1'-{2-[(5R)-3-[3,5-bis(trifluoromethyl)benzoyl]-5-(4-fluorophenyl)-1,3-oxazolidin-5-yl]ethyl}-2,3-dihydrospiro[indene-1,4'-piperidin]-2-yl]oxy}acetyl)(methyl)amino]butanoate

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