6-oxo-6-(4'-(4-(undec-10-enoyloxy)benzoyloxy)biphenyl-4-yloxy)hexanoic acid

Base Information

Chemical Name:6-oxo-6-(4'-(4-(undec-10-enoyloxy)benzoyloxy)biphenyl-4-yloxy)hexanoic acid
CAS No.:1246517-82-7
Molecular Formula:C₃₆H₄₀O₈
Molecular Weight:600.709
Hs Code.:

Synonyms:6-oxo-6-(4'-(4-(undec-10-enoyloxy)benzoyloxy)biphenyl-4-yloxy)hexanoic acid

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Chemical Property of 6-oxo-6-(4'-(4-(undec-10-enoyloxy)benzoyloxy)biphenyl-4-yloxy)hexanoic acid

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Technology Process of 6-oxo-6-(4'-(4-(undec-10-enoyloxy)benzoyloxy)biphenyl-4-yloxy)hexanoic acid

There total 1 articles about 6-oxo-6-(4'-(4-(undec-10-enoyloxy)benzoyloxy)biphenyl-4-yloxy)hexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 753458-21-8
4'-hydroxybiphenyl-4-yl 4-(undec-10-enoyloxy)benzoate

: 111-50-2
Adipic acid dichloride

: 1246517-82-7
6-oxo-6-(4'-(4-(undec-10-enoyloxy)benzoyloxy)biphenyl-4-yloxy)hexanoic acid

Guidance literature:: 4'-hydroxybiphenyl-4-yl 4-(undec-10-enoyloxy)benzoate; Adipic acid dichloride; With pyridine; In chloroform; at 65 ℃;

With sulfuric acid; water; at 20 ℃;
DOI:10.1016/j.polymer.2011.09.002

Reference yield:

: 1246517-82-7
6-oxo-6-(4'-(4-(undec-10-enoyloxy)benzoyloxy)biphenyl-4-yloxy)hexanoic acid

: 1246517-83-8
4'-(6-chloro-6-oxohexanoyloxy)biphenyl-4-yl 4-(undec-10-enoyloxy)benzoate

Guidance literature:: With pyridine; thionyl chloride; In tetrahydrofuran; at 20 - 60 ℃;
DOI:10.1016/j.polymer.2011.09.002

Reference yield:

: 1246517-82-7
6-oxo-6-(4'-(4-(undec-10-enoyloxy)benzoyloxy)biphenyl-4-yloxy)hexanoic acid

: 4'-(4-(undec-10-enoyloxy)benzoyloxy)biphenyl-4-yl 6-(perfluorooctanoyloxy)hexahydrofuro[3,2-b]furan-3-yl adipate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; thionyl chloride / tetrahydrofuran / 20 - 60 °C

2: pyridine / tetrahydrofuran / 65 °C

3: pyridine / tetrahydrofuran / 63 °C

With pyridine; thionyl chloride; In tetrahydrofuran;
DOI:10.1016/j.polymer.2011.09.002