(Z)-(S)-2-((S)-2-Benzyloxycarbonylamino-2-carboxy-ethylsulfanyl)-5-hydroxy-hex-2-enoic acid methyl ester

Base Information

Chemical Name:(Z)-(S)-2-((S)-2-Benzyloxycarbonylamino-2-carboxy-ethylsulfanyl)-5-hydroxy-hex-2-enoic acid methyl ester
CAS No.:98051-43-5
Molecular Formula:C₁₈H₂₃NO₇S
Molecular Weight:397.449
Hs Code.:

Synonyms:(Z)-(S)-2-((S)-2-Benzyloxycarbonylamino-2-carboxy-ethylsulfanyl)-5-hydroxy-hex-2-enoic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-(S)-2-((S)-2-Benzyloxycarbonylamino-2-carboxy-ethylsulfanyl)-5-hydroxy-hex-2-enoic acid methyl ester

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Technology Process of (Z)-(S)-2-((S)-2-Benzyloxycarbonylamino-2-carboxy-ethylsulfanyl)-5-hydroxy-hex-2-enoic acid methyl ester

There total 16 articles about (Z)-(S)-2-((S)-2-Benzyloxycarbonylamino-2-carboxy-ethylsulfanyl)-5-hydroxy-hex-2-enoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 105729-46-2
(Z)-(S)-2-((R)-2-Benzyloxycarbonylamino-2-tert-butoxycarbonyl-ethylsulfanyl)-5-hydroxy-hex-2-enoic acid methyl ester

: 98051-43-5
(Z)-(S)-2-((R)-2-Benzyloxycarbonylamino-2-carboxy-ethylsulfanyl)-5-hydroxy-hex-2-enoic acid methyl ester

Guidance literature:: With trifluoroacetic acid; for 0.916667h;
DOI:10.1021/jo00376a052

Reference yield: 67.0%

: 98051-42-4
(Z)-(S)-2-((S)-2-Benzhydryloxycarbonyl-2-benzyloxycarbonylamino-ethylsulfanyl)-5-(tetrahydro-pyran-2-yloxy)-hex-2-enoic acid methyl ester

: 98051-43-5
(Z)-(S)-2-((S)-2-Benzyloxycarbonylamino-2-carboxy-ethylsulfanyl)-5-hydroxy-hex-2-enoic acid methyl ester

Guidance literature:: With hydrogenchloride; In 1,2-dimethoxyethane; at 65 ℃;
DOI:10.1021/jo00219a064

Reference yield:

: 6081-61-4
N-(benzyloxycarbonyl)-D-serine

: 98051-43-5
(Z)-(S)-2-((S)-2-Benzyloxycarbonylamino-2-carboxy-ethylsulfanyl)-5-hydroxy-hex-2-enoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

2: 1.) CH₃SO₂Cl₂, Et₃N, 2.) NaI / 2.) acetone

3: 1.) NaH, DMSO / 1.) THF, -78 deg C, 2.) THF, -15 deg C

4: 67 percent / 1 N aq. HCl / 1,2-dimethoxy-ethane / 65 °C

With hydrogenchloride; sodium hydride; dimethyl sulfoxide; triethylamine; sodium iodide; In 1,2-dimethoxyethane;
DOI:10.1021/jo00219a064