d₁-2-methoxy-1-phenyl-1H-indene

Base Information

Chemical Name:d₁-2-methoxy-1-phenyl-1H-indene
CAS No.:1610735-69-7
Molecular Formula:C₁₆H₁₄O
Molecular Weight:223.279
Hs Code.:

d<SUB>1</SUB>-2-methoxy-1-phenyl-1H-indene

Synonyms:d₁-2-methoxy-1-phenyl-1H-indene

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Chemical Property of d₁-2-methoxy-1-phenyl-1H-indene

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Technology Process of d₁-2-methoxy-1-phenyl-1H-indene

There total 6 articles about d₁-2-methoxy-1-phenyl-1H-indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1610735-63-1
d₁-1-ethynyl-2-(methoxy(phenyl)methyl)benzene

: 1610735-69-7
d₁-2-methoxy-1-phenyl-1H-indene

: d₁-2-methoxy-3-phenyl-1H-indene

Guidance literature:: With 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; silver(I) triflimide; In 1,2-dichloro-ethane; at 28 ℃; for 4h; chemoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1002/adsc.201300988

Reference yield:

: 38274-16-7
2-bromo-1-(trimethylsilylethynyl)benzene

: 1610735-69-7
d₁-2-methoxy-1-phenyl-1H-indene

: d₁-2-methoxy-3-phenyl-1H-indene

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -78 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 - 28 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.2: 1.5 h / 0 °C / Inert atmosphere

4.1: potassium carbonate / methanol; dichloromethane

5.1: 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; silver(I) triflimide / 1,2-dichloro-ethane / 4 h / 28 °C / Inert atmosphere; Molecular sieve

With n-butyllithium; 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; sodium hydride; potassium carbonate; silver(I) triflimide; In tetrahydrofuran; methanol; hexane; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/adsc.201300988

Reference yield:

: 2-((trimethylsilyl)ethynyl-d)benzaldehyde

: 1610735-69-7
d₁-2-methoxy-1-phenyl-1H-indene

: d₁-2-methoxy-3-phenyl-1H-indene

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 - 28 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 1.5 h / 0 °C / Inert atmosphere

3.1: potassium carbonate / methanol; dichloromethane

4.1: 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; silver(I) triflimide / 1,2-dichloro-ethane / 4 h / 28 °C / Inert atmosphere; Molecular sieve

With n-butyllithium; 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; sodium hydride; potassium carbonate; silver(I) triflimide; In tetrahydrofuran; methanol; hexane; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/adsc.201300988