2,3,7,8,12,18-hexamethyl-5-(4-azidomethylphenyl)-13,17-diethylporphyrinato zinc(II)

Base Information

• Chemical Name: 2,3,7,8,12,18-hexamethyl-5-(4-azidomethylphenyl)-13,17-diethylporphyrinato zinc(II)
• CAS No.: 1220106-18-2
• Molecular Formula: C₃₇H₃₇N₇Zn
• Molecular Weight: 645.138

Synonyms:2,3,7,8,12,18-hexamethyl-5-(4-azidomethylphenyl)-13,17-diethylporphyrinato zinc(II)

Chemical Property of 2,3,7,8,12,18-hexamethyl-5-(4-azidomethylphenyl)-13,17-diethylporphyrinato zinc(II)

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Technology Process of 2,3,7,8,12,18-hexamethyl-5-(4-azidomethylphenyl)-13,17-diethylporphyrinato zinc(II)

There total 2 articles about 2,3,7,8,12,18-hexamethyl-5-(4-azidomethylphenyl)-13,17-diethylporphyrinato zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,3,7,8,12,18-hexamethyl-5-(4-azidomethylphenyl)-13,17-diethylporphyrin → 2,3,7,8,12,18-hexamethyl-5-(4-azidomethylphenyl)-13,17-diethylporphyrinato zinc(II) (1220106-18-2)

Guidance literature:

With zinc(II) acetate tetrahydrate; sodium acetate; In methanol; chloroform; for 1.5h; Reflux;

DOI:10.1021/ja100192x

Reference yield: 91.0%

zinc(II) acetate tetrahydrate + 2,3,7,8,12,18-hexamethyl-5-(4-azidomethylphenyl)-13,17-diethylporphyrin → 2,3,7,8,12,18-hexamethyl-5-(4-azidomethylphenyl)-13,17-diethylporphyrinato zinc(II) (1220106-18-2)

Guidance literature:

With sodium acetate; In methanol; chloroform; dissolving Zn salt and ligand in CHCl3/methanol, reflux for 90 min in the presence of sodium acetate; evapn. in vac., dissolving in CH2Cl2, washing with water, drying (MgSO4), evapn. in vac., column chromy. (silica, CH2Cl2), evapn.;

DOI:10.1021/ja100192x

Reference yield: 46.0%

2,3,7,8,12,18-hexamethyl-5-(4-azidomethylphenyl)-13,17-diethylporphyrinato zinc(II) (1220106-18-2) + 1,9-(4-((4-vinylphenoxy)methyl)-ethynyl)-2,6-diethyl-1,7-dimethyl-8-(p-methylbenzoyl)-BDP → 3,5-(8,12-diethyl-2,3,7,13,17,18-hexamethyl-20,-para((4-((4-vinylphenoxy)methyl)-triazole)-N-benzyl)zinc bisporphyrin)-2,6-die...

Guidance literature:

With CuI; DIPEA; In dichloromethane; Ar; in dark B compd. (0.051 mmol) and Zn compd. (0.133 mmol) in DCM; CuI(0.053 mmol) and DIPEa (0.116 mmol) added, stirred at room temp. for 7 h; washed (H2O), org. layer dried (MgSO4), evapd., chromd. (DCM/MeCN=90/10), evapd., elem. anal.;

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