meso-methyl 5-epi-quinate

Base Information

Chemical Name:meso-methyl 5-epi-quinate
CAS No.:193956-42-2
Molecular Formula:C₈H₁₄O₆
Molecular Weight:206.196
Hs Code.:

Synonyms:meso-methyl 5-epi-quinate

Suppliers and Price of meso-methyl 5-epi-quinate

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Chemical Property of meso-methyl 5-epi-quinate

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Technology Process of meso-methyl 5-epi-quinate

There total 11 articles about meso-methyl 5-epi-quinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 193888-33-4
methyl 3,4-O-cyclohexylidene-epi-quinate

: 193956-42-2
meso-methyl 5-epi-quinate

Guidance literature:: With trifluoroacetic acid; In water; for 0.5h; Ambient temperature;
DOI:10.1016/S0040-4039(97)01109-X

Reference yield:

: 193888-32-3
3,4-O-cyclohexylidene-5-oxoquinate

: 193956-42-2
meso-methyl 5-epi-quinate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / sodium borohydride / methanol / 0.5 h / -30 °C

2: 93 percent / trifluoroacetic acid / H₂O / 0.5 h / Ambient temperature

With sodium tetrahydroborate; trifluoroacetic acid; In methanol; water;
DOI:10.1016/S0040-4039(97)01109-X

Reference yield:

: 77-95-2
D-(-)-quinic acid

: 193956-42-2
meso-methyl 5-epi-quinate

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / p-toluenesulfonic acid / toluene / 7 h / Heating

2: 80 percent / methanol / 5 h / Ambient temperature

3: 92 percent / Dess-Martin oxidation / CH₂Cl₂ / 2 h / Ambient temperature

4: 90 percent / sodium borohydride / methanol / 0.5 h / -30 °C

5: 93 percent / trifluoroacetic acid / H₂O / 0.5 h / Ambient temperature

With sodium tetrahydroborate; Dess-Martin periodane; toluene-4-sulfonic acid; trifluoroacetic acid; In methanol; dichloromethane; water; toluene;
DOI:10.1016/S0040-4039(97)01109-X