4-{2,4-bis[4-(9H-carbazol-9-yl)phenyl]-7H-pyrrolo[2,3-d]pyrimidin-7-yl}-N,N-diphenylaniline

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Chemical Name:4-{2,4-bis[4-(9H-carbazol-9-yl)phenyl]-7H-pyrrolo[2,3-d]pyrimidin-7-yl}-N,N-diphenylaniline
CAS No.:1334106-98-7
Molecular Formula:C₆₀H₄₀N₆
Molecular Weight:845.018
Hs Code.:

Synonyms:4-{2,4-bis[4-(9H-carbazol-9-yl)phenyl]-7H-pyrrolo[2,3-d]pyrimidin-7-yl}-N,N-diphenylaniline

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Chemical Property of 4-{2,4-bis[4-(9H-carbazol-9-yl)phenyl]-7H-pyrrolo[2,3-d]pyrimidin-7-yl}-N,N-diphenylaniline

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Technology Process of 4-{2,4-bis[4-(9H-carbazol-9-yl)phenyl]-7H-pyrrolo[2,3-d]pyrimidin-7-yl}-N,N-diphenylaniline

There total 4 articles about 4-{2,4-bis[4-(9H-carbazol-9-yl)phenyl]-7H-pyrrolo[2,3-d]pyrimidin-7-yl}-N,N-diphenylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1236078-17-3
2,4-di(4-(9H-carbazol-9-yl)phenyl)-7H-pyrrolo[2,3-d]pyrimidine

: 36809-26-4
4-N,N-diphenylamino-1-bromobenzene

: 1334106-98-7
4-{2,4-bis[4-(9H-carbazol-9-yl)phenyl]-7H-pyrrolo[2,3-d]pyrimidin-7-yl}-N,N-diphenylaniline

Guidance literature:: With potassium phosphate; copper(l) iodide; trans-1,2-Diaminocyclohexane; In 1,4-dioxane; for 29h; Inert atmosphere;
DOI:10.1016/j.tet.2011.10.040

Reference yield: 59.0%

: 1236078-17-3
2,4-di(4-(9H-carbazol-9-yl)phenyl)-7H-pyrrolo[2,3-d]pyrimidine

: 38257-52-2
4-(N,N-diphenylamino)iodobenzene

: 1334106-98-7
4-{2,4-bis[4-(9H-carbazol-9-yl)phenyl]-7H-pyrrolo[2,3-d]pyrimidin-7-yl}-N,N-diphenylaniline

Guidance literature:: 2,4-di(4-(9H-carbazol-9-yl)phenyl)-7H-pyrrolo[2,3-d]pyrimidine; With potassium phosphate; copper(l) iodide; In 1,4-dioxane; Inert atmosphere;

4-(N,N-diphenylamino)iodobenzene; With trans-1,2-Diaminocyclohexane; In 1,4-dioxane; for 29h; Inert atmosphere; Reflux;
DOI:10.1055/s-0030-1260931

Reference yield:

: 419536-33-7
4-(carbazol-9-yl)phenylboronic acid

: 1334106-98-7
4-{2,4-bis[4-(9H-carbazol-9-yl)phenyl]-7H-pyrrolo[2,3-d]pyrimidin-7-yl}-N,N-diphenylaniline

Guidance literature:: Multi-step reaction with 2 steps

2.1: copper(l) iodide; potassium phosphate / 1,4-dioxane / Inert atmosphere

2.2: 29 h / Inert atmosphere; Reflux

With potassium phosphate; copper(l) iodide; In 1,4-dioxane; 1.1: Suzuki coupling;
DOI:10.1055/s-0030-1260931