C₃₂H₃₃N₅O₃

Base Information

Chemical Name:C₃₂H₃₃N₅O₃
CAS No.:1187313-12-7
Molecular Formula:C₃₂H₃₃N₅O₃
Molecular Weight:535.646
Hs Code.:

C<sub>32</sub>H<sub>33</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₃₂H₃₃N₅O₃

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Chemical Property of C₃₂H₃₃N₅O₃

Chemical Property:

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Technology Process of C₃₂H₃₃N₅O₃

There total 11 articles about C₃₂H₃₃N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187313-22-9
4-(6-bromopyrazolo[1,5-a]pyrimidin-3-yl)quinoline

: 1187313-10-5
tert-butyl 4-methoxy-4-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)piperidine-1-carboxylate

: 1187313-12-7
C₃₂H₃₃N₅O₃

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 150 ℃; Inert atmosphere; Microwave irradiation;

Reference yield:

: 4363-93-3
quinoline-4-carboxaldehyde

: 1187313-12-7
C₃₂H₃₃N₅O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: methanol; sodium tetrahydroborate / 1.33 h / 0 - 20 °C

2.1: thionyl chloride / dichloromethane / 2.33 h / 0 - 20 °C

2.2: pH > 7 / Saturated solution

3.1: N,N-dimethyl-formamide / 20 - 80 °C

4.1: 6 h / 120 °C

5.1: hydrazine monohydrobromide / ethanol; water / 5 h / 110 °C

5.2: Saturated solution

6.1: acetic acid / ethanol / 5 h / 50 °C

7.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 150 °C / Inert atmosphere; Microwave irradiation

With methanol; sodium tetrahydroborate; thionyl chloride; hydrazine monohydrobromide; potassium carbonate; acetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 5632-17-7
4-(chloromethyl)quinoline

: 1187313-12-7
C₃₂H₃₃N₅O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N-dimethyl-formamide / 20 - 80 °C

2.1: 6 h / 120 °C

3.1: hydrazine monohydrobromide / ethanol; water / 5 h / 110 °C

3.2: Saturated solution

4.1: acetic acid / ethanol / 5 h / 50 °C

5.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 150 °C / Inert atmosphere; Microwave irradiation

With hydrazine monohydrobromide; potassium carbonate; acetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;