sulfuric acid mono-{2-[7-acetylamino-6-(2-allyloxy-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy]-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl} ester

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Chemical Name:sulfuric acid mono-{2-[7-acetylamino-6-(2-allyloxy-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy]-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl} ester
CAS No.:253336-92-4
Molecular Formula:C₃₀H₄₃NO₁₉S
Molecular Weight:753.733
Hs Code.:

sulfuric acid mono-{2-[7-acetylamino-6-(2-allyloxy-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-2-phenyl-hexahydro-pyrano[3,2-<i>d</i>][1,3]dioxin-8-yloxy]-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl} ester

Synonyms:sulfuric acid mono-{2-[7-acetylamino-6-(2-allyloxy-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy]-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl} ester

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Chemical Property of sulfuric acid mono-{2-[7-acetylamino-6-(2-allyloxy-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy]-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl} ester

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Technology Process of sulfuric acid mono-{2-[7-acetylamino-6-(2-allyloxy-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy]-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl} ester

There total 9 articles about sulfuric acid mono-{2-[7-acetylamino-6-(2-allyloxy-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy]-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 253336-91-3
2,2-dimethyl-propionic acid 6-{7-acetylamino-6-[2-allyloxy-6-(2,2-dimethyl-propionyloxymethyl)-3,5-dihydroxy-tetrahydro-pyran-4-yloxy]-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy}-3,5-dihydroxy-4-sulfooxy-tetrahydro-pyran-2-ylmethyl ester

: 253336-92-4
sulfuric acid mono-{2-[7-acetylamino-6-(2-allyloxy-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy]-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl} ester

Guidance literature:: With methanol; sodium methylate; at 20 ℃; for 2h;
DOI:10.1016/S0960-894X(99)00507-7

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 253336-92-4
sulfuric acid mono-{2-[7-acetylamino-6-(2-allyloxy-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy]-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl} ester

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / p-TsOH / acetonitrile / 0.67 h / 20 °C

2: 70 percent / Hg(CN)2; HgBr₂; MS 4A / 1,2-dichloro-ethane / 18 h / 40 - 45 °C

3: 90 percent / 1M MeONa/MeOH / CH₂Cl₂ / 0.33 h / -10 - -5 °C / pH 10

4: 85 percent / SO₃*pyridine / 6 h / 0 - 5 °C

5: 100 percent / MeONa; MeOH / 2 h / 20 °C

With methanol; pyridine-SO₃ complex; sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; mercury dibromide; In dichloromethane; 1,2-dichloro-ethane; acetonitrile; 1: transacetalization / 2: Condensation / 3: Deacetylation / 4: Substitution / 5: deprotection;
DOI:10.1016/S0960-894X(99)00507-7

Reference yield:

: 10378-06-0,20757-53-3,35954-65-5,123483-77-2,134308-33-1
2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyranoso)[1,2-d]-2-oxazoline

: 253336-92-4
sulfuric acid mono-{2-[7-acetylamino-6-(2-allyloxy-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy]-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl} ester

Guidance literature:: Multi-step reaction with 7 steps

1: 50 percent / BF₃*Et₂O; MS 4A / CH₂Cl₂ / 4 h / 20 °C

2: 90 percent / 1M MeONa/MeOH / CH₂Cl₂ / 0.33 h / -10 - -5 °C / pH 10

3: 85 percent / p-TsOH / acetonitrile / 0.67 h / 20 °C

4: 70 percent / Hg(CN)2; HgBr₂; MS 4A / 1,2-dichloro-ethane / 18 h / 40 - 45 °C

5: 90 percent / 1M MeONa/MeOH / CH₂Cl₂ / 0.33 h / -10 - -5 °C / pH 10

6: 85 percent / SO₃*pyridine / 6 h / 0 - 5 °C

7: 100 percent / MeONa; MeOH / 2 h / 20 °C

With methanol; pyridine-SO₃ complex; boron trifluoride diethyl etherate; sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; mercury dibromide; In dichloromethane; 1,2-dichloro-ethane; acetonitrile; 1: glycosylation / 2: Deacetylation / 3: transacetalization / 4: Condensation / 5: Deacetylation / 6: Substitution / 7: deprotection;
DOI:10.1016/S0960-894X(99)00507-7