Sodium; [4-(2-mercaptomethyl-3-phenyl-propionylamino)-phenyl]-methanesulfonate

Base Information

Chemical Name:Sodium; [4-(2-mercaptomethyl-3-phenyl-propionylamino)-phenyl]-methanesulfonate
CAS No.:138063-41-9
Molecular Formula:C₁₇H₁₈NO₄S₂*Na
Molecular Weight:387.456
Hs Code.:

Synonyms:Sodium; [4-(2-mercaptomethyl-3-phenyl-propionylamino)-phenyl]-methanesulfonate

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Chemical Property of Sodium; [4-(2-mercaptomethyl-3-phenyl-propionylamino)-phenyl]-methanesulfonate

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Technology Process of Sodium; [4-(2-mercaptomethyl-3-phenyl-propionylamino)-phenyl]-methanesulfonate

There total 5 articles about Sodium; [4-(2-mercaptomethyl-3-phenyl-propionylamino)-phenyl]-methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 116112-34-6
Sodium; [4-(2-acetylsulfanylmethyl-3-phenyl-propionylamino)-phenyl]-methanesulfonate

: 138063-41-9
Sodium; [4-(2-mercaptomethyl-3-phenyl-propionylamino)-phenyl]-methanesulfonate

Guidance literature:: With sodium hydroxide; In water; for 0.5h; Ambient temperature;
DOI:10.1021/jm00081a024

Reference yield:

: 5669-19-2
2-Benzyl-2-propenoic acid

: 138063-41-9
Sodium; [4-(2-mercaptomethyl-3-phenyl-propionylamino)-phenyl]-methanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: 1 h / 80 °C

2: SOCl₂ / CHCl₃; dimethylformamide / 0.5 h / Heating

3: aq. NaOH / tetrahydrofuran / 0.5 h / Ambient temperature

4: 69 percent / 1N aq. NaOH / H₂O / 0.5 h / Ambient temperature

With sodium hydroxide; thionyl chloride; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00081a024

Reference yield:

: 6387-28-6
(4-aminophenyl)methanesulfonic acid

: 138063-41-9
Sodium; [4-(2-mercaptomethyl-3-phenyl-propionylamino)-phenyl]-methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / tetrahydrofuran / 0.5 h / Ambient temperature

2: 69 percent / 1N aq. NaOH / H₂O / 0.5 h / Ambient temperature

With sodium hydroxide; In tetrahydrofuran; water;
DOI:10.1021/jm00081a024