Technology Process of C40H50N6O5
There total 13 articles about C40H50N6O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 1 h / Heating / reflux
2: sodium hydrogencarbonate / water / 20 °C
3: sodium tetrahydroborate / tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 1 h / 0 °C
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
With
sodium tetrahydroborate; thionyl chloride; sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
tetrakis(triphenylphosphine) palladium(0); N,N-dimethyl-formamide;
In
tetrahydrofuran; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydrogencarbonate / water / 20 °C
2: sodium tetrahydroborate / tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 1 h / 0 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
With
sodium tetrahydroborate; sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; dichloromethane; water;