15-(benzyloxy-carbonyloctadecyl-amino)-pentadecyl-β-D-2,3,4,6-tetra-O-acetylmanno-pyranoside

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Chemical Name:15-(benzyloxy-carbonyloctadecyl-amino)-pentadecyl-β-D-2,3,4,6-tetra-O-acetylmanno-pyranoside
CAS No.:454472-14-1
Molecular Formula:C₅₅H₉₃NO₁₂
Molecular Weight:960.343
Hs Code.:

Synonyms:15-(benzyloxy-carbonyloctadecyl-amino)-pentadecyl-β-D-2,3,4,6-tetra-O-acetylmanno-pyranoside

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Chemical Property of 15-(benzyloxy-carbonyloctadecyl-amino)-pentadecyl-β-D-2,3,4,6-tetra-O-acetylmanno-pyranoside

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Technology Process of 15-(benzyloxy-carbonyloctadecyl-amino)-pentadecyl-β-D-2,3,4,6-tetra-O-acetylmanno-pyranoside

There total 4 articles about 15-(benzyloxy-carbonyloctadecyl-amino)-pentadecyl-β-D-2,3,4,6-tetra-O-acetylmanno-pyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 273737-80-7
(15-hydroxy-pentadecyl)-octadecyl carbamic acid benzyl ester

: 4163-60-4
β-D-galactose peracetate

: 454472-14-1
15-(benzyloxy-carbonyloctadecyl-amino)-pentadecyl-β-D-2,3,4,6-tetra-O-acetylmanno-pyranoside

Guidance literature:: β-D-galactose peracetate; With tin(IV) chloride; In acetonitrile; at 0 ℃; for 0.5h;

(15-hydroxy-pentadecyl)-octadecyl carbamic acid benzyl ester; In acetonitrile; at 20 ℃; for 5h;
DOI:10.1016/S0960-894X(02)00200-7

Reference yield:

: 76529-42-5
methyl 15-hydroxypentadecanoate

: 454472-14-1
15-(benzyloxy-carbonyloctadecyl-amino)-pentadecyl-β-D-2,3,4,6-tetra-O-acetylmanno-pyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: 100 percent / 148 °C

2.1: 97 percent / LiAlH₄ / tetrahydrofuran / 10 h / 20 °C

3.1: 70 percent / Et₃N / CH₂Cl₂ / 20 °C

4.1: SnCl₄ / acetonitrile / 0.5 h / 0 °C

4.2: 69 percent / acetonitrile / 5 h / 20 °C

With lithium aluminium tetrahydride; tin(IV) chloride; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/S0960-894X(02)00200-7

Reference yield:

: 273737-78-3
15-hydroxy-pentadecanoic acid octadecylamide

: 454472-14-1
15-(benzyloxy-carbonyloctadecyl-amino)-pentadecyl-β-D-2,3,4,6-tetra-O-acetylmanno-pyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 97 percent / LiAlH₄ / tetrahydrofuran / 10 h / 20 °C

2.1: 70 percent / Et₃N / CH₂Cl₂ / 20 °C

3.1: SnCl₄ / acetonitrile / 0.5 h / 0 °C

3.2: 69 percent / acetonitrile / 5 h / 20 °C

With lithium aluminium tetrahydride; tin(IV) chloride; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/S0960-894X(02)00200-7