Technology Process of C31H47F3N2O13
There total 7 articles about C31H47F3N2O13 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanesulfonic acid; sodium cyanoborohydride;
In
tetrahydrofuran;
for 4h;
Molecular sieve;
DOI:10.1016/j.tetlet.2013.06.065
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium methylate / methanol / 16 h
1.2: 5 h / 40 °C
2.1: triethylamine / methanol / 3 h
2.2: 16 h
3.1: sodium cyanoborohydride; methanesulfonic acid / tetrahydrofuran / 4 h / Molecular sieve
With
methanesulfonic acid; sodium methylate; sodium cyanoborohydride; triethylamine;
In
tetrahydrofuran; methanol;
1.2: |Staudinger Azide Reduction;
DOI:10.1016/j.tetlet.2013.06.065
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium azide / N,N-dimethyl-formamide / 15 h / 75 °C
2.1: N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate / dichloromethane / 1 h / -20 °C / Molecular sieve
3.1: ethylenediamine; i-Amyl alcohol / 4 h / 140 °C / Reflux
4.1: pyridine / 1.5 h / Reflux
5.1: sodium methylate / methanol / 16 h
5.2: 5 h / 40 °C
6.1: triethylamine / methanol / 3 h
6.2: 16 h
7.1: sodium cyanoborohydride; methanesulfonic acid / tetrahydrofuran / 4 h / Molecular sieve
With
pyridine; N-iodo-succinimide; sodium azide; methanesulfonic acid; i-Amyl alcohol; triethylsilyl trifluoromethyl sulfonate; sodium methylate; sodium cyanoborohydride; ethylenediamine; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
5.2: |Staudinger Azide Reduction;
DOI:10.1016/j.tetlet.2013.06.065
