N-(benzyloxycarbonyl)-L-alanyl-O-(2-acetamide-3-O-benzyl-2-deoxy-α-D-galactopyranosyl)-L-threonyl-L-alanine benzyl ester

Base Information

Chemical Name:N-(benzyloxycarbonyl)-L-alanyl-O-(2-acetamide-3-O-benzyl-2-deoxy-α-D-galactopyranosyl)-L-threonyl-L-alanine benzyl ester
CAS No.:766521-27-1
Molecular Formula:C₄₀H₅₀N₄O₁₂
Molecular Weight:778.857
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)-L-alanyl-O-(2-acetamide-3-O-benzyl-2-deoxy-α-D-galactopyranosyl)-L-threonyl-L-alanine benzyl ester

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Chemical Property of N-(benzyloxycarbonyl)-L-alanyl-O-(2-acetamide-3-O-benzyl-2-deoxy-α-D-galactopyranosyl)-L-threonyl-L-alanine benzyl ester

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Technology Process of N-(benzyloxycarbonyl)-L-alanyl-O-(2-acetamide-3-O-benzyl-2-deoxy-α-D-galactopyranosyl)-L-threonyl-L-alanine benzyl ester

There total 4 articles about N-(benzyloxycarbonyl)-L-alanyl-O-(2-acetamide-3-O-benzyl-2-deoxy-α-D-galactopyranosyl)-L-threonyl-L-alanine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: N-(benzyloxycarbonyl)-L-alanyl-O-(2-acetamide-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl)-L-threonyl-L-alanine benzyl ester

: 766521-27-1
N-(benzyloxycarbonyl)-L-alanyl-O-(2-acetamide-3-O-benzyl-2-deoxy-α-D-galactopyranosyl)-L-threonyl-L-alanine benzyl ester

Guidance literature:: With camphor-10-sulfonic acid; In methanol; for 3h;
DOI:10.1021/ma049756z

Reference yield:

: N-(benzyloxycarbonyl)-L-alanyl-O-(2-azide-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl)-L-threonyl-L-alanine benzyl ester

: 766521-27-1
N-(benzyloxycarbonyl)-L-alanyl-O-(2-acetamide-3-O-benzyl-2-deoxy-α-D-galactopyranosyl)-L-threonyl-L-alanine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / pyridine / 20 h / 20 °C

2: 100 percent / CSA / methanol / 3 h

With pyridine; camphor-10-sulfonic acid; In methanol;
DOI:10.1021/ma049756z

Reference yield:

: 2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-galactopyranosyl fluoride

: 766521-27-1
N-(benzyloxycarbonyl)-L-alanyl-O-(2-acetamide-3-O-benzyl-2-deoxy-α-D-galactopyranosyl)-L-threonyl-L-alanine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: SnCl₂; AgClO₄; 4 Angstroem molecular sieves / CH₂Cl₂ / 3 h / 20 °C

1.2: 53 percent / CH₂Cl₂ / 96 h / -20 - 20 °C

2.1: 70 percent / pyridine / 20 h / 20 °C

3.1: 100 percent / CSA / methanol / 3 h

With pyridine; 4 A molecular sieve; camphor-10-sulfonic acid; silver perchlorate; tin(ll) chloride; In methanol; dichloromethane;
DOI:10.1021/ma049756z