N-[1-(7-benzenesulfonyl-6-iodo-7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-4-ylmethyl]-4-tert-butylbenzamide

Base Information

Chemical Name:N-[1-(7-benzenesulfonyl-6-iodo-7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-4-ylmethyl]-4-tert-butylbenzamide
CAS No.:1607005-60-6
Molecular Formula:C₂₉H₃₂IN₅O₃S
Molecular Weight:657.575
Hs Code.:

Synonyms:N-[1-(7-benzenesulfonyl-6-iodo-7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-4-ylmethyl]-4-tert-butylbenzamide

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Chemical Property of N-[1-(7-benzenesulfonyl-6-iodo-7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-4-ylmethyl]-4-tert-butylbenzamide

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Technology Process of N-[1-(7-benzenesulfonyl-6-iodo-7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-4-ylmethyl]-4-tert-butylbenzamide

There total 2 articles about N-[1-(7-benzenesulfonyl-6-iodo-7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-4-ylmethyl]-4-tert-butylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 876343-09-8
7-(benzenesulfonyl)-4-chloro-6-iodo-7H-pyrrolo[2,3-d]pyrimidine

: 1016746-93-2
4-tert-butyl-N-piperidin-4-ylmethylbenzamide

: 1607005-60-6
N-[1-(7-benzenesulfonyl-6-iodo-7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-4-ylmethyl]-4-tert-butylbenzamide

Guidance literature:: With triethylamine; In ethanol; at 80 ℃; for 2h;

Reference yield:

: 1607005-59-3
4-[(4-tert-butylbenzoylamino)methyl]piperidine-1-carboxylic acid tert-butyl ester

: 1607005-60-6
N-[1-(7-benzenesulfonyl-6-iodo-7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidin-4-ylmethyl]-4-tert-butylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

2: triethylamine / ethanol / 2 h / 80 °C

With triethylamine; trifluoroacetic acid; In ethanol; dichloromethane;