(2R,1'R,,2'S,5'R)-5'-methyl-2'-(1-methyl-1-phenylethyl)cyclohexyl 1,2,3,4-tetrahydro-4-oxo-2-phenylpyridine-1-carboxylate

Base Information

Chemical Name:(2R,1'R,,2'S,5'R)-5'-methyl-2'-(1-methyl-1-phenylethyl)cyclohexyl 1,2,3,4-tetrahydro-4-oxo-2-phenylpyridine-1-carboxylate
CAS No.:126378-50-5
Molecular Formula:C₂₈H₃₃NO₃
Molecular Weight:431.575
Hs Code.:

Synonyms:(2R,1'R,,2'S,5'R)-5'-methyl-2'-(1-methyl-1-phenylethyl)cyclohexyl 1,2,3,4-tetrahydro-4-oxo-2-phenylpyridine-1-carboxylate

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Chemical Property of (2R,1'R,,2'S,5'R)-5'-methyl-2'-(1-methyl-1-phenylethyl)cyclohexyl 1,2,3,4-tetrahydro-4-oxo-2-phenylpyridine-1-carboxylate

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Technology Process of (2R,1'R,,2'S,5'R)-5'-methyl-2'-(1-methyl-1-phenylethyl)cyclohexyl 1,2,3,4-tetrahydro-4-oxo-2-phenylpyridine-1-carboxylate

There total 13 articles about (2R,1'R,,2'S,5'R)-5'-methyl-2'-(1-methyl-1-phenylethyl)cyclohexyl 1,2,3,4-tetrahydro-4-oxo-2-phenylpyridine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 126378-58-3
2(S)-phenyl-1-<((1R,2S,5R)-8-phenylmenthoxy)carbonyl>-5-(triisopropylsilyl)-2,3-dihydro-4-pyridone

: 126378-50-5
(2R,1'R,,2'S,5'R)-5'-methyl-2'-(1-methyl-1-phenylethyl)cyclohexyl 1,2,3,4-tetrahydro-4-oxo-2-phenylpyridine-1-carboxylate

Guidance literature:: With hydrogen bromide; acetic acid; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/ja00090a019

Reference yield: 76.0%

: 126378-43-6
(1R,2S,5R)-(-)-8-phenylmenthyl chloroformate

: 157379-62-9
(2R)-2,3-dihydro-2-phenylpyridin-4(1H)-one

: 126378-50-5
(2R,1'R,,2'S,5'R)-5'-methyl-2'-(1-methyl-1-phenylethyl)cyclohexyl 1,2,3,4-tetrahydro-4-oxo-2-phenylpyridine-1-carboxylate

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; 1.) 15 min.;
DOI:10.1002/hlca.19950780106

Reference yield:

: 65253-04-5
(-)-8-phenylmenthol

: 126378-50-5
(2R,1'R,,2'S,5'R)-5'-methyl-2'-(1-methyl-1-phenylethyl)cyclohexyl 1,2,3,4-tetrahydro-4-oxo-2-phenylpyridine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / quinoline / toluene / 16 h / Ambient temperature

2: 1.) toluene, -23 deg C, 15 min, 2.) toluene, THF, -78 deg C, 1 h

With quinoline; In toluene;
DOI:10.1021/ja00090a019