(2R,5R)-2-(3,4-dimethoxyphenyl)-5-(3,4-methylenedioxyphenyl)-3,4-dimethylenetetrahydrofuran

Base Information

Chemical Name:(2R,5R)-2-(3,4-dimethoxyphenyl)-5-(3,4-methylenedioxyphenyl)-3,4-dimethylenetetrahydrofuran
CAS No.:1201328-27-9
Molecular Formula:C₂₁H₂₀O₅
Molecular Weight:352.387
Hs Code.:

Synonyms:(2R,5R)-2-(3,4-dimethoxyphenyl)-5-(3,4-methylenedioxyphenyl)-3,4-dimethylenetetrahydrofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,5R)-2-(3,4-dimethoxyphenyl)-5-(3,4-methylenedioxyphenyl)-3,4-dimethylenetetrahydrofuran

Chemical Property:

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Technology Process of (2R,5R)-2-(3,4-dimethoxyphenyl)-5-(3,4-methylenedioxyphenyl)-3,4-dimethylenetetrahydrofuran

There total 2 articles about (2R,5R)-2-(3,4-dimethoxyphenyl)-5-(3,4-methylenedioxyphenyl)-3,4-dimethylenetetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₈O₁₁S₂

: 1201328-27-9
(2R,5R)-2-(3,4-dimethoxyphenyl)-5-(3,4-methylenedioxyphenyl)-3,4-dimethylenetetrahydrofuran

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; In N,N-dimethyl-formamide; at 80 ℃; for 3h;
DOI:10.1271/bbb.90107

Reference yield:

: C₂₃H₂₈O₁₁S₂

: 1201328-27-9
(2R,5R)-2-(3,4-dimethoxyphenyl)-5-(3,4-methylenedioxyphenyl)-3,4-dimethylenetetrahydrofuran

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; In N,N-dimethyl-formamide; at 80 ℃; for 3h;
DOI:10.1271/bbb.90107

Reference yield: 47.0%

: 1201328-27-9
(2R,5R)-2-(3,4-dimethoxyphenyl)-5-(3,4-methylenedioxyphenyl)-3,4-dimethylenetetrahydrofuran

: 1201327-00-5
(7S,7'S,8S,8'S)-3',4'-dimethoxy-3,4-methylenedioxylignane-9,9'-diol

Guidance literature:: (2R,5R)-2-(3,4-dimethoxyphenyl)-5-(3,4-methylenedioxyphenyl)-3,4-dimethylenetetrahydrofuran; With dimethylsulfide borane complex; In tetrahydrofuran; at 20 ℃; for 1h; Cooling with ice;

With dihydrogen peroxide; sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 ℃; for 2h; stereoselective reaction;
DOI:10.1271/bbb.90107