allyl (3-O-acetyl-2-deoxy-4,6-O-isopropylidene-2-trichloroacetamido-8-D-glucopyranosyl)-(1→2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→3)]-(4-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:allyl (3-O-acetyl-2-deoxy-4,6-O-isopropylidene-2-trichloroacetamido-8-D-glucopyranosyl)-(1→2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→3)]-(4-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside
CAS No.:1091625-93-2
Molecular Formula:C₈₄H₉₄Cl₃NO₂₂
Molecular Weight:1576.02
Hs Code.:

allyl (3-O-acetyl-2-deoxy-4,6-O-isopropylidene-2-trichloroacetamido-8-D-glucopyranosyl)-(1→2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→3)]-(4-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Synonyms:allyl (3-O-acetyl-2-deoxy-4,6-O-isopropylidene-2-trichloroacetamido-8-D-glucopyranosyl)-(1→2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→3)]-(4-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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Chemical Property of allyl (3-O-acetyl-2-deoxy-4,6-O-isopropylidene-2-trichloroacetamido-8-D-glucopyranosyl)-(1→2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→3)]-(4-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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Technology Process of allyl (3-O-acetyl-2-deoxy-4,6-O-isopropylidene-2-trichloroacetamido-8-D-glucopyranosyl)-(1→2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→3)]-(4-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

There total 1 articles about allyl (3-O-acetyl-2-deoxy-4,6-O-isopropylidene-2-trichloroacetamido-8-D-glucopyranosyl)-(1→2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→3)]-(4-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 428818-08-0
3,4,6-tri-O-acetyl-2-deoxy-2-trichloroacetamido-α/β-D-glucopyranose trichloroacetimidate

: 1091625-51-2
allyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1->3)-(4-O-benzyl-α-L-rhamnopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

: 1091625-93-2
allyl (3-O-acetyl-2-deoxy-4,6-O-isopropylidene-2-trichloroacetamido-8-D-glucopyranosyl)-(1→2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→3)]-(4-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With trifluorormethanesulfonic acid; In toluene; at -40 - 20 ℃; Molecular sieve;
DOI:10.1021/jo802127z

Reference yield: 79.0%

: 1091625-93-2
allyl (3-O-acetyl-2-deoxy-4,6-O-isopropylidene-2-trichloroacetamido-8-D-glucopyranosyl)-(1→2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→3)]-(4-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

: 1091625-94-3
allyl (2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl)-(1->2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1->3)]-(4-O-benzyl-α-L-rhamnopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: allyl (3-O-acetyl-2-deoxy-4,6-O-isopropylidene-2-trichloroacetamido-8-D-glucopyranosyl)-(1→2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→3)]-(4-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside; With methanol; sodium methylate; at 20 ℃; for 3h;

In methanol;
DOI:10.1021/jo802127z

Reference yield:

: 1091625-93-2
allyl (3-O-acetyl-2-deoxy-4,6-O-isopropylidene-2-trichloroacetamido-8-D-glucopyranosyl)-(1→2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→3)]-(4-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

: C₇₆H₈₉NO₁₈

Guidance literature:: allyl (3-O-acetyl-2-deoxy-4,6-O-isopropylidene-2-trichloroacetamido-8-D-glucopyranosyl)-(1→2)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→3)]-(4-O-benzyl-α-L-rhamnopyranosyl)-(1→2)-3,4-di-O-benzyl-α-L-rhamnopyranoside; With methanol; sodium methylate; In dichloromethane; at 20 ℃; for 3h;

In methanol;
DOI:10.1021/jo802127z