2'-deoxy-N⁶-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{O^P-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N⁶,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine

Base Information

• Chemical Name: 2'-deoxy-N⁶-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{O^P-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N⁶,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine
• CAS No.: 153120-95-7
• Molecular Formula: C₆₁H₅₆N₁₃O₂₀P
• Molecular Weight: 1322.16

Synonyms:2'-deoxy-N⁶-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{O^P-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N⁶,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine

Chemical Property of 2'-deoxy-N⁶-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{O^P-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N⁶,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine

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Technology Process of 2'-deoxy-N⁶-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{O^P-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N⁶,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine

There total 1 articles about 2'-deoxy-N⁶-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{O^P-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N⁶,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2'-deoxy-5'-O-(dimethoxytrityl)-N6-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{OP-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N6,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine (153155-01-2) → 2'-deoxy-N6-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{OP-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N6,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine (153120-95-7)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1002/hlca.200390186

Reference yield: 96.0%

2'-deoxy-5'-O-(4-monomethoxytrityl)-N6-[2-(4-nitrophenyl)ethoxycarbonyl]adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite] + 2'-deoxy-N6-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{OP-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N6,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine (153120-95-7) → C108H98N20O32P2

Guidance literature:

2'-deoxy-5'-O-(4-monomethoxytrityl)-N⁶-[2-(4-nitrophenyl)ethoxycarbonyl]adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite]; 2'-deoxy-N⁶-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{O^P-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N⁶,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine; With 1H-tetrazole; In dichloromethane; acetonitrile; at 20 ℃; for 2h;

With pyridine; iodine; In various solvents; for 0.25h;

DOI:10.1002/hlca.200390186

Reference yield: 93.0%

2'-deoxy-N6,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite] (153120-91-3) + 2'-deoxy-N6-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{OP-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N6,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine (153120-95-7) → C97H89N21O35P2 (153120-96-8)

Guidance literature:

2'-deoxy-N⁶,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine 3'-[2-(4-nitrophenyl)ethyl diisopropylphosphoramidite]; 2'-deoxy-N⁶-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{O^P-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N⁶,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine; With 1H-tetrazole; In dichloromethane; acetonitrile; at 20 ℃; for 2h;

With pyridine; iodine; In various solvents; for 0.25h;

DOI:10.1002/hlca.200390186

upstream raw materials:

2'-deoxy-5'-O-(dimethoxytrityl)-N⁶-[(9H-fluoren-9-ylmethoxy)carbonyl]adenylyl-{3'-{O^P-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N⁶,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine

Downstream raw materials:

C₉₇H₈₉N₂₁O₃₅P₂

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