Technology Process of C38H58O13
There total 8 articles about C38H58O13 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: triethylamine / dichloromethane / 4 h / 0 - 20 °C
2.1: tetrabutylammomium bromide; sodium hydroxide / water / 40 h / 70 °C
3.1: water; acetic acid / 12 h / 25 °C
4.1: triethylamine / dichloromethane
5.1: sodium iodide / 1,2-dimethoxyethane
6.1: dimethylsulfide borane complex / tetrahydrofuran / 20 h / 0 °C
6.2: 3 h / 25 °C
7.1: sodium hydride / tetrahydrofuran / 12 h / 0 - 25 °C
8.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 15 h / 25 °C
9.1: tetrabutylammomium bromide; sodium hydroxide / water / 30 h / 60 °C
With
dimethylsulfide borane complex; palladium 10% on activated carbon; tetrabutylammomium bromide; water; hydrogen; sodium hydride; acetic acid; triethylamine; sodium iodide; sodium hydroxide;
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; ethyl acetate;
DOI:10.1016/j.tetlet.2011.09.139
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydride / tetrahydrofuran / 12 h / 0 - 25 °C
2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 15 h / 25 °C
3: tetrabutylammomium bromide; sodium hydroxide / water / 30 h / 60 °C
With
palladium 10% on activated carbon; tetrabutylammomium bromide; hydrogen; sodium hydride; sodium hydroxide;
In
tetrahydrofuran; water; ethyl acetate;
DOI:10.1016/j.tetlet.2011.09.139
