N-2.6-Dimethylaminoisopropylaldimin

Base Information

• Chemical Name: N-2.6-Dimethylaminoisopropylaldimin
• CAS No.: 68294-66-6
• Molecular Formula: C₁₂H₁₇N
• Molecular Weight: 175.274
• Mol file: 68294-66-6.mol

Synonyms:N-2.6-Dimethylaminoisopropylaldimin

Chemical Property of N-2.6-Dimethylaminoisopropylaldimin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-2.6-Dimethylaminoisopropylaldimin

There total 4 articles about N-2.6-Dimethylaminoisopropylaldimin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) + diisopropyl zinc (625-81-0) → N-2.6-Dimethylaminoisopropylaldimin (68294-66-6)

Guidance literature:

In toluene; at 95 ℃; for 2h;

DOI:10.1021/jo00252a069

Reference yield:

N-Isobutyl-N-trimethylsilyl-2.6-dimethylanilin (68294-59-7) → N-2.6-Dimethylaminoisopropylaldimin (68294-66-6)

Guidance literature:

In methanol;

Reference yield:

2,6-dimethylphenyl isonitrile (119072-54-7,2769-71-3) → N-2.6-Dimethylaminoisopropylaldimin (68294-66-6)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) benzene, Et₂O, (ii) /BRN= 1209232/

2: 277 - 290 °C

3: methanol

In methanol;

upstream raw materials:

N-Isobutyl-N-trimethylsilyl-2.6-dimethylanilin

2,6-dimethylphenyl isonitrile

diisopropyl zinc

<2-methyl-1(2,6-xylylimino)propyl>trimethylsilane