C₃₃H₄₇IO₅

Base Information

Chemical Name:C₃₃H₄₇IO₅
CAS No.:1618093-06-3
Molecular Formula:C₃₃H₄₇IO₅
Molecular Weight:650.638
Hs Code.:

C<sub>33</sub>H<sub>47</sub>IO<sub>5</sub>

Synonyms:C₃₃H₄₇IO₅

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Chemical Property of C₃₃H₄₇IO₅

Chemical Property:

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Technology Process of C₃₃H₄₇IO₅

There total 9 articles about C₃₃H₄₇IO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₈H₅₇IO₆

: 1618093-06-3
C₃₃H₄₇IO₅

Guidance literature:: C₃₈H₅₇IO₆; With hydrogenchloride; water; In tetrahydrofuran; at 50 ℃; Inert atmosphere;

With iodine; In toluene; Inert atmosphere; Reflux;
DOI:10.1021/jo501266g

Reference yield:

: 1618092-85-5
2-[4-bromo-2-((2-ethylhexyl)oxy)-5-methoxyphenyl]-5,5-dimethyl-1,3-dioxane

: 1618093-06-3
C₃₃H₄₇IO₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Glovebox; Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: trifluoroacetic acid / tetrahydrofuran; water / 50 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

4.1: water; hydrogenchloride / tetrahydrofuran / 50 °C / Inert atmosphere

4.2: Inert atmosphere; Reflux

With hydrogenchloride; n-butyllithium; potassium tert-butylate; water; trifluoroacetic acid; In tetrahydrofuran; hexane; water; 3.1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo501266g

Reference yield:

: 150-76-5
4-methoxy-phenol

: 1618093-06-3
C₃₃H₄₇IO₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere

2.1: potassium acetate; bromine / acetic acid / 50 °C / Inert atmosphere

3.1: sodium hydroxide; water / tert-butyl alcohol / Inert atmosphere; Reflux

4.1: triethylamine; magnesium chloride / acetonitrile / Inert atmosphere; Reflux

5.1: toluene-4-sulfonic acid / toluene / Inert atmosphere; Dean-Stark; Reflux

6.1: potassium hydroxide / dimethyl sulfoxide / 50 °C / Inert atmosphere

7.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Glovebox; Inert atmosphere

7.2: -78 - 20 °C / Inert atmosphere

8.1: trifluoroacetic acid / tetrahydrofuran; water / 50 °C / Inert atmosphere

9.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

10.1: water; hydrogenchloride / tetrahydrofuran / 50 °C / Inert atmosphere

10.2: Inert atmosphere; Reflux

With hydrogenchloride; n-butyllithium; potassium tert-butylate; water; bromine; potassium acetate; toluene-4-sulfonic acid; triethylamine; trifluoroacetic acid; potassium hydroxide; sodium hydroxide; magnesium chloride; In tetrahydrofuran; hexane; water; acetic acid; dimethyl sulfoxide; toluene; acetonitrile; tert-butyl alcohol; 6.1: |Williamson Ether Synthesis / 9.1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo501266g