17-hydroxy-10,13-dimethyl-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-3H-cyclopenta[a]phenanthren-3-one

Base Information

• Chemical Name: 17-hydroxy-10,13-dimethyl-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-3H-cyclopenta[a]phenanthren-3-one
• CAS No.: 1221910-14-0
• Molecular Formula: C₁₉H₂₈O₂
• Molecular Weight: 288.43
• Mol file: 1221910-14-0.mol

Synonyms:17-Hydroxy-10,13-dimethyl-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-cyclopenta[a]phenanthren-3-one

Chemical Property of 17-hydroxy-10,13-dimethyl-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-3H-cyclopenta[a]phenanthren-3-one

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

14-HYDROXY-2,15-DIMETHYLTETRACYCLO[8.7.0.0(2,7).0(11,15)]HEPTADEC-6-EN-5-ONE 95.00% ^*data from reagent suppliers

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Technology Process of 17-hydroxy-10,13-dimethyl-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-3H-cyclopenta[a]phenanthren-3-one

There total 1 articles about 17-hydroxy-10,13-dimethyl-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-3H-cyclopenta[a]phenanthren-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 17-Hydroxy-10,13-dimethyl-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-cyclopenta[a]phenanthren-3-one (1221910-14-0)

Guidance literature:

entspr. Semicarbazon, Titanouschlorid;

Reference yield: 84.0%

17-Hydroxy-10,13-dimethyl-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-cyclopenta[a]phenanthren-3-one (1221910-14-0) → 4,5-Epoxy-testosteron (2189-83-5,6765-87-3,16318-53-9,17503-06-9,17503-07-0,17597-25-0,51154-10-0)

Guidance literature:

With Oxone; ammonium bicarbonate; In water; acetonitrile; at 20 ℃; for 2h;

DOI:10.1021/ol801157m

Reference yield: 62.0%

17-Hydroxy-10,13-dimethyl-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-cyclopenta[a]phenanthren-3-one (1221910-14-0) + manganese(II) benzoate (636-13-5,17375-29-0) → Benzoic acid 17-hydroxy-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-2-yl ester (122723-65-3)

Guidance literature:

With manganese triacetate; In benzene; for 30h; Heating;

DOI:10.1021/jo00278a006

Downstream raw materials:

1,4-diazabicyclo<2.2.2>octane radical cation

Benzoic acid 17-hydroxy-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-2-yl ester

4,5-Epoxy-testosteron

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