p-nitrophenyl (3-azido-3-deoxy-β-D-glucopyranosyl)-(1->3)-(β-D-glucopyranosyl)-(1->3)-β-D-glucopyranoside

Base Information

Chemical Name:p-nitrophenyl (3-azido-3-deoxy-β-D-glucopyranosyl)-(1->3)-(β-D-glucopyranosyl)-(1->3)-β-D-glucopyranoside
CAS No.:593281-71-1
Molecular Formula:C₂₄H₃₄N₄O₁₇
Molecular Weight:650.551
Hs Code.:

Synonyms:p-nitrophenyl (3-azido-3-deoxy-β-D-glucopyranosyl)-(1->3)-(β-D-glucopyranosyl)-(1->3)-β-D-glucopyranoside

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Chemical Property of p-nitrophenyl (3-azido-3-deoxy-β-D-glucopyranosyl)-(1->3)-(β-D-glucopyranosyl)-(1->3)-β-D-glucopyranoside

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Technology Process of p-nitrophenyl (3-azido-3-deoxy-β-D-glucopyranosyl)-(1->3)-(β-D-glucopyranosyl)-(1->3)-β-D-glucopyranoside

There total 3 articles about p-nitrophenyl (3-azido-3-deoxy-β-D-glucopyranosyl)-(1->3)-(β-D-glucopyranosyl)-(1->3)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2492-87-7
4-nitrophenyl-β-D-glucoside

: 593281-66-4
(3-azido-3-deoxy-β-D-glucopyranosyl)-(1->3)-α-D-glucopyranosyl fluoride

: 593281-71-1
p-nitrophenyl (3-azido-3-deoxy-β-D-glucopyranosyl)-(1->3)-(β-D-glucopyranosyl)-(1->3)-β-D-glucopyranoside

Guidance literature:: With mutated (1,3)-β-D-glucan endohydrolase Glu231Gly; In phosphate buffer; at 37 ℃; pH=7.0;
DOI:10.1002/chem.200304733

Reference yield:

: 593281-70-0
(2,4,6-tri-O-acetyl-3-azido-3-deoxy-β-D-glucopyranosyl)-(1->3)-2,4,6-tri-O-acetyl-α-D-glucopyranosyl fluoride

: 593281-71-1
p-nitrophenyl (3-azido-3-deoxy-β-D-glucopyranosyl)-(1->3)-(β-D-glucopyranosyl)-(1->3)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / NaOMe / methanol / 2 h / 0 - 20 °C

2: 81 percent / mutated (1,3)-β-D-glucan endohydrolase Glu231Gly / aq. phosphate buffer / 37 °C / pH 7.0

With mutated (1,3)-β-D-glucan endohydrolase Glu231Gly; sodium methylate; In methanol; phosphate buffer;
DOI:10.1002/chem.200304733

Reference yield:

: (2,4,6-tri-O-acetyl-3-azido-3-deoxy-β-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-D-glucopyranose

: 593281-71-1
p-nitrophenyl (3-azido-3-deoxy-β-D-glucopyranosyl)-(1->3)-(β-D-glucopyranosyl)-(1->3)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / HF; pyridine / 12 h / 4 °C

2: 99 percent / NaOMe / methanol / 2 h / 0 - 20 °C

3: 81 percent / mutated (1,3)-β-D-glucan endohydrolase Glu231Gly / aq. phosphate buffer / 37 °C / pH 7.0

With pyridine; mutated (1,3)-β-D-glucan endohydrolase Glu231Gly; hydrogen fluoride; sodium methylate; In methanol; phosphate buffer;
DOI:10.1002/chem.200304733