4,4'-(dithieno[2,3-a:3',2'-c]phenazine-8,11-diyl)bis(N,N-diphenylaniline)

Base Information

Chemical Name:4,4'-(dithieno[2,3-a:3',2'-c]phenazine-8,11-diyl)bis(N,N-diphenylaniline)
CAS No.:1446275-71-3
Molecular Formula:C₅₂H₃₄N₄S₂
Molecular Weight:779.001
Hs Code.:

Synonyms:4,4'-(dithieno[2,3-a:3',2'-c]phenazine-8,11-diyl)bis(N,N-diphenylaniline)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-(dithieno[2,3-a:3',2'-c]phenazine-8,11-diyl)bis(N,N-diphenylaniline)

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Technology Process of 4,4'-(dithieno[2,3-a:3',2'-c]phenazine-8,11-diyl)bis(N,N-diphenylaniline)

There total 3 articles about 4,4'-(dithieno[2,3-a:3',2'-c]phenazine-8,11-diyl)bis(N,N-diphenylaniline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1446275-72-4
8,11-dibromodithieno[2,3-a:3',2'-c]phenazine

: 201802-67-7
4-(diphenylamino)phenyl boronic acid

: 1446275-71-3
4,4'-(dithieno[2,3-a:3',2'-c]phenazine-8,11-diyl)bis(N,N-diphenylaniline)

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; Reflux; Inert atmosphere;
DOI:10.1021/ol4012025

Reference yield:

: 69272-50-0
1,2-diamine-3,6-dibromobenzene

: 1446275-71-3
4,4'-(dithieno[2,3-a:3',2'-c]phenazine-8,11-diyl)bis(N,N-diphenylaniline)

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / ethanol / Reflux; Inert atmosphere

2: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / Reflux; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; acetic acid; In tetrahydrofuran; ethanol; water; 2: |Suzuki Coupling;
DOI:10.1021/ol4012025

Reference yield:

: 15155-41-6
4,7-dibromobenzo[c][1,2,5]thiadiazole

: 1446275-71-3
4,4'-(dithieno[2,3-a:3',2'-c]phenazine-8,11-diyl)bis(N,N-diphenylaniline)

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / ethanol

2: acetic acid / ethanol / Reflux; Inert atmosphere

3: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / Reflux; Inert atmosphere

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; acetic acid; In tetrahydrofuran; ethanol; water; 3: |Suzuki Coupling;
DOI:10.1021/ol4012025