N-{1-[(4-chlorophenyl)methyl]-1H-pyrazol-3-yl}-5-[1-(3,5-dimethyl-1H-pyrazol-1-yl)ethyl]-1,3,4-thiadiazol-2-amine

Base Information

Chemical Name:N-{1-[(4-chlorophenyl)methyl]-1H-pyrazol-3-yl}-5-[1-(3,5-dimethyl-1H-pyrazol-1-yl)ethyl]-1,3,4-thiadiazol-2-amine
CAS No.:1251929-09-5
Molecular Formula:C₁₉H₂₀ClN₇S
Molecular Weight:413.934
Hs Code.:

Synonyms:N-{1-[(4-chlorophenyl)methyl]-1H-pyrazol-3-yl}-5-[1-(3,5-dimethyl-1H-pyrazol-1-yl)ethyl]-1,3,4-thiadiazol-2-amine

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Chemical Property of N-{1-[(4-chlorophenyl)methyl]-1H-pyrazol-3-yl}-5-[1-(3,5-dimethyl-1H-pyrazol-1-yl)ethyl]-1,3,4-thiadiazol-2-amine

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Technology Process of N-{1-[(4-chlorophenyl)methyl]-1H-pyrazol-3-yl}-5-[1-(3,5-dimethyl-1H-pyrazol-1-yl)ethyl]-1,3,4-thiadiazol-2-amine

There total 3 articles about N-{1-[(4-chlorophenyl)methyl]-1H-pyrazol-3-yl}-5-[1-(3,5-dimethyl-1H-pyrazol-1-yl)ethyl]-1,3,4-thiadiazol-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1251930-22-9
C₁₉H₂₂ClN₇OS

: 1251929-09-5
N-{1-[(4-chlorophenyl)methyl]-1H-pyrazol-3-yl}-5-[1-(3,5-dimethyl-1H-pyrazol-1-yl)ethyl]-1,3,4-thiadiazol-2-amine

Guidance literature:: C₁₉H₂₂ClN₇OS; With sulfuric acid; at 20 ℃; for 1.5h;

With ammonia; In water; Cooling with ice;

Reference yield:

: 500335-74-0
ethyl 2-(3,5-dimethyl-1H-pyrazol-1-yl)propanoate

: 1251929-09-5
N-{1-[(4-chlorophenyl)methyl]-1H-pyrazol-3-yl}-5-[1-(3,5-dimethyl-1H-pyrazol-1-yl)ethyl]-1,3,4-thiadiazol-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrazine hydrate / ethanol; water / 16 h / 50 °C

2.1: dichloromethane / 1.5 h

3.1: sulfuric acid / 1.5 h / 20 °C

3.2: Cooling with ice

With sulfuric acid; hydrazine hydrate; In ethanol; dichloromethane; water;

Reference yield:

: 1251929-87-9
2-(3,5-dimethyl-1H-pyrazol-1-yl)propanohydrazide

: 588695-59-4
C₁₁H₈ClN₃S

: 1251929-09-5
N-{1-[(4-chlorophenyl)methyl]-1H-pyrazol-3-yl}-5-[1-(3,5-dimethyl-1H-pyrazol-1-yl)ethyl]-1,3,4-thiadiazol-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 1.5 h

2.1: sulfuric acid / 1.5 h / 20 °C

2.2: Cooling with ice

With sulfuric acid; In dichloromethane;