4'-methyl-4-nitro-α,β-dihydrochalcone

Base Information

• Chemical Name: 4'-methyl-4-nitro-α,β-dihydrochalcone
• CAS No.: 35031-90-4
• Molecular Formula: C₁₆H₁₅NO₃
• Molecular Weight: 269.3
• Mol file: 35031-90-4.mol

Synonyms:4'-methyl-4-nitro-α,β-dihydrochalcone

Chemical Property of 4'-methyl-4-nitro-α,β-dihydrochalcone

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 4'-methyl-4-nitro-α,β-dihydrochalcone

There total 3 articles about 4'-methyl-4-nitro-α,β-dihydrochalcone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-(4-methylphenyl)-2-propen-1-ol (58824-48-9) + 4-nitrophenylboronic acid (24067-17-2) → 4'-methyl-4-nitro-α,β-dihydrochalcone (35031-90-4)

Guidance literature:

With 2.9-dimethyl-1,10-phenanthroline; palladium diacetate; copper(l) chloride; In dimethyl sulfoxide; at 50 ℃; for 12h; under 760.051 Torr;

DOI:10.1039/c3gc42504e

Reference yield: 79.0%

3-(4-nitrophenyl)-1-p-tolylprop-2-en-1-one (102692-40-0,102692-55-7,13736-56-6) → 4'-methyl-4-nitro-α,β-dihydrochalcone (35031-90-4)

Guidance literature:

With D-glucose; sodium chloride; In water; acetone; at 28 ℃; for 24h; Reagent/catalyst; Microbiological reaction;

DOI:10.1039/c8ra04669g

Reference yield:

→ 4'-methyl-4-nitro-α,β-dihydrochalcone (35031-90-4)

Guidance literature:

aus Hydrozimtsaeure 7, (H3PO4)n;

upstream raw materials:

1-(4-methylphenyl)-2-propen-1-ol

4-nitrophenylboronic acid

3-(4-nitrophenyl)-1-p-tolylprop-2-en-1-one