cis-(-)-N-<(4',7',7'-trimethyl-3'-oxo-2'-oxabicyclo<2.2.1>heptyl)-1'-carbonyl>-8a-phenyldecahydroquinoline

Base Information

Chemical Name:cis-(-)-N-<(4',7',7'-trimethyl-3'-oxo-2'-oxabicyclo<2.2.1>heptyl)-1'-carbonyl>-8a-phenyldecahydroquinoline
CAS No.:131556-12-2
Molecular Formula:C₂₅H₃₃NO₃
Molecular Weight:395.542
Hs Code.:

Synonyms:cis-(-)-N-<(4',7',7'-trimethyl-3'-oxo-2'-oxabicyclo<2.2.1>heptyl)-1'-carbonyl>-8a-phenyldecahydroquinoline

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Chemical Property of cis-(-)-N-<(4',7',7'-trimethyl-3'-oxo-2'-oxabicyclo<2.2.1>heptyl)-1'-carbonyl>-8a-phenyldecahydroquinoline

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Technology Process of cis-(-)-N-<(4',7',7'-trimethyl-3'-oxo-2'-oxabicyclo<2.2.1>heptyl)-1'-carbonyl>-8a-phenyldecahydroquinoline

There total 5 articles about cis-(-)-N-<(4',7',7'-trimethyl-3'-oxo-2'-oxabicyclo<2.2.1>heptyl)-1'-carbonyl>-8a-phenyldecahydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1074-06-2
Δ^1(8a)-octahydroquinoline

: 131556-12-2
cis-(-)-N-<(4',7',7'-trimethyl-3'-oxo-2'-oxabicyclo<2.2.1>heptyl)-1'-carbonyl>-8a-phenyldecahydroquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / diethyl ether / 2 h / Heating

2: pyridine / CH₂Cl₂; diethyl ether / 3 h / Ambient temperature

With pyridine; In diethyl ether; dichloromethane;
DOI:10.1021/jm00087a020

Reference yield:

: 1125-99-1
1-(1-Cyclohexen-1-yl)pyrrolidine

: 131556-12-2
cis-(-)-N-<(4',7',7'-trimethyl-3'-oxo-2'-oxabicyclo<2.2.1>heptyl)-1'-carbonyl>-8a-phenyldecahydroquinoline

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / dioxane / 1.5 h / Heating

2: LiAlH₄ / diethyl ether / 0.5 h / Ambient temperature

3: aq. NaOH / 1 h / 100 °C

4: 50 percent / diethyl ether / 2 h / Heating

5: pyridine / CH₂Cl₂; diethyl ether / 3 h / Ambient temperature

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; In 1,4-dioxane; diethyl ether; dichloromethane;
DOI:10.1021/jm00087a020

Reference yield:

: 4697-90-9
3-(2-pyrrolidino-cyclohex-1-enyl)-propionitrile

: 131556-12-2
cis-(-)-N-<(4',7',7'-trimethyl-3'-oxo-2'-oxabicyclo<2.2.1>heptyl)-1'-carbonyl>-8a-phenyldecahydroquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: LiAlH₄ / diethyl ether / 0.5 h / Ambient temperature

2: aq. NaOH / 1 h / 100 °C

3: 50 percent / diethyl ether / 2 h / Heating

4: pyridine / CH₂Cl₂; diethyl ether / 3 h / Ambient temperature

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; In diethyl ether; dichloromethane;
DOI:10.1021/jm00087a020