4-Chloro-benzenesulfonic acid; compound with p-tolylamine

Base Information

• Chemical Name: 4-Chloro-benzenesulfonic acid; compound with p-tolylamine
• CAS No.: 53039-73-9
• Molecular Formula: C₆H₅ClO₃S*C₇H₉N
• Molecular Weight: 299.778
• Mol file: 53039-73-9.mol

Synonyms:4-Chloro-benzenesulfonic acid; compound with p-tolylamine

Chemical Property of 4-Chloro-benzenesulfonic acid; compound with p-tolylamine

Chemical Property:

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Technology Process of 4-Chloro-benzenesulfonic acid; compound with p-tolylamine

There total 11 articles about 4-Chloro-benzenesulfonic acid; compound with p-tolylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl chlorobenzene-p-sulphonate (20443-71-4) + p-toluidine (106-49-0,12221-03-3) → 4-Chloro-benzenesulfonic acid; compound with p-tolylamine (53039-73-9) + N-ethyl-p-tolylamine (622-57-1)

Guidance literature:

In methanol; at 65 ℃;

Reference yield:

methyl p-chlorobenzenesulphonate (15481-45-5) + p-toluidine (106-49-0,12221-03-3) → N-methyl-p-toluidine (623-08-5) + 4-Chloro-benzenesulfonic acid; compound with p-tolylamine (53039-73-9)

Guidance literature:

In methanol; at 65 ℃;

Reference yield:

p-toluidine (106-49-0,12221-03-3) + 5-bromoindan-2-yl chlorobenzene-p-sulfonate → 4-Chloro-benzenesulfonic acid; compound with p-tolylamine (53039-73-9) + (5-Bromo-indan-2-yl)-p-tolyl-amine

Guidance literature:

In methanol; at 55 ℃; Rate constant;

DOI:10.1039/P29930002415

upstream raw materials:

ethyl chlorobenzene-p-sulphonate

p-toluidine

methyl p-chlorobenzenesulphonate

4-Chloro-benzenesulfonic acid 1-methyl-1-phenyl-ethyl ester