3,3’-[(1,3-dioxo-1,3-propanediyl)diimino]bis[5-(aminocarbonyl)-2,4,6-triiodobenzoyl chloride]

Base Information

Chemical Name:3,3’-[(1,3-dioxo-1,3-propanediyl)diimino]bis[5-(aminocarbonyl)-2,4,6-triiodobenzoyl chloride]
CAS No.:134768-77-7
Molecular Formula:C₁₉H₈Cl₂I₆N₄O₆
Molecular Weight:1220.63
Hs Code.:

Synonyms:3,3’-[(1,3-dioxo-1,3-propanediyl)diimino]bis[5-(aminocarbonyl)-2,4,6-triiodobenzoyl chloride]

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Chemical Property of 3,3’-[(1,3-dioxo-1,3-propanediyl)diimino]bis[5-(aminocarbonyl)-2,4,6-triiodobenzoyl chloride]

Chemical Property:

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Technology Process of 3,3’-[(1,3-dioxo-1,3-propanediyl)diimino]bis[5-(aminocarbonyl)-2,4,6-triiodobenzoyl chloride]

There total 5 articles about 3,3’-[(1,3-dioxo-1,3-propanediyl)diimino]bis[5-(aminocarbonyl)-2,4,6-triiodobenzoyl chloride] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 134768-76-6
3-amino-5-(aminocarbonyl)-2,4,6-triiodobenzoyl chloride

: 141-82-2
malonic acid

: 134768-77-7
3,3’-[(1,3-dioxo-1,3-propanediyl)diimino]bis[5-(aminocarbonyl)-2,4,6-triiodobenzoyl chloride]

: 3-carbamoyl-5-(3-chloro-3-oxopropanamido)-2,4,6-triiodobenzoyl chloride

: 872117-60-7
3-(aminocarbonyl)-5-[[3-[[3-(aminocarbonyl)-5-(chlorocarbonyl)-2,4,6-triiodophenyl]amino]-1,3-dioxopropyl]amino]-2,4,6-triiodobenzoic acid

Guidance literature:: With phosphorus trichloride; In 1,2-dimethoxyethane; for 4.16667 - 4.25h; Product distribution / selectivity; Heating / reflux;

Reference yield: 92.4%

: 134768-76-6
3-amino-5-(aminocarbonyl)-2,4,6-triiodobenzoyl chloride

: 141-82-2
malonic acid

: 134768-77-7
3,3’-[(1,3-dioxo-1,3-propanediyl)diimino]bis[5-(aminocarbonyl)-2,4,6-triiodobenzoyl chloride]

Guidance literature:: With trichlorophosphate; In tetrahydrofuran; at 45 - 50 ℃; for 20h; Reagent/catalyst; Temperature;

Reference yield:

: C₈H₈N₂O₃*H₃N

: 134768-77-7
3,3’-[(1,3-dioxo-1,3-propanediyl)diimino]bis[5-(aminocarbonyl)-2,4,6-triiodobenzoyl chloride]

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; sodium iodine dichloride / water / 60 - 80 °C / Large scale

2: thionyl chloride / ethyl acetate; N,N-dimethyl-formamide / 6 h / Reflux

3: trichlorophosphate / tetrahydrofuran / 20 h / 45 - 50 °C

With hydrogenchloride; thionyl chloride; sodium iodine dichloride; trichlorophosphate; In tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide;